3-t-butyl-6-methyl-2,3,4,5-tetrahydrobenzyl alcohol

Base Information

Chemical Name:3-t-butyl-6-methyl-2,3,4,5-tetrahydrobenzyl alcohol
CAS No.:75646-64-9
Molecular Formula:C₁₂H₂₂O
Molecular Weight:182.306
Hs Code.:

Synonyms:3-t-butyl-6-methyl-2,3,4,5-tetrahydrobenzyl alcohol

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Chemical Property of 3-t-butyl-6-methyl-2,3,4,5-tetrahydrobenzyl alcohol

Chemical Property:

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Technology Process of 3-t-butyl-6-methyl-2,3,4,5-tetrahydrobenzyl alcohol

There total 11 articles about 3-t-butyl-6-methyl-2,3,4,5-tetrahydrobenzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 75646-62-7
3-t-butyl-6-methyl-2,3,4,5-tetrahydrobenzaldehyde

: 75646-64-9
3-t-butyl-6-methyl-2,3,4,5-tetrahydrobenzyl alcohol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at -10 ℃; for 0.75h;

Reference yield:

: 67001-73-4,31845-19-9
4-(tert-butyl)cyclohex-1-ene-1-carboxylic acid

: 75646-64-9
3-t-butyl-6-methyl-2,3,4,5-tetrahydrobenzyl alcohol

Guidance literature:: Multi-step reaction with 8 steps

1: 100 percent / pyridine, oxalyl chloride / benzene / 1 h / Ambient temperature

2: 99 percent / benzene / 18 h / Heating

3: 94 percent / AlCl₃, LiAlH₄ / diethyl ether / 1.) 0 deg C, 1.5 h, 2.) RT, 18 h

4: dimethylsulfoxide / 18 h / 45 °C

5: 92 percent / potassium t-butoxide / tetrahydrofuran / 2 h / -10 °C

6: 30percent oxalic acid / tetrahydrofuran / 0.08 h / Heating

7: KOH / methanol / 4 h / Ambient temperature

8: 95 percent / LiAlH₄ / diethyl ether / 0.75 h / -10 °C

With pyridine; potassium hydroxide; lithium aluminium tetrahydride; aluminium trichloride; oxalyl dichloride; potassium tert-butylate; oxalic acid; In tetrahydrofuran; methanol; diethyl ether; dimethyl sulfoxide; benzene;

Reference yield:

: 31673-51-5
4-tert-butyl-1,5-cyclohexadiene-1-carboxylic acid

: 75646-64-9
3-t-butyl-6-methyl-2,3,4,5-tetrahydrobenzyl alcohol

Guidance literature:: Multi-step reaction with 10 steps

1: 99 percent / Li / liquid ammonia; diethyl ether / 0.25 h / -70 °C

2: 67 percent / NaOH / H₂O; ethane-1,2-diol / 45 h / Heating

3: 100 percent / pyridine, oxalyl chloride / benzene / 1 h / Ambient temperature

4: 99 percent / benzene / 18 h / Heating

5: 94 percent / AlCl₃, LiAlH₄ / diethyl ether / 1.) 0 deg C, 1.5 h, 2.) RT, 18 h

6: dimethylsulfoxide / 18 h / 45 °C

7: 92 percent / potassium t-butoxide / tetrahydrofuran / 2 h / -10 °C

8: 30percent oxalic acid / tetrahydrofuran / 0.08 h / Heating

9: KOH / methanol / 4 h / Ambient temperature

10: 95 percent / LiAlH₄ / diethyl ether / 0.75 h / -10 °C

With pyridine; potassium hydroxide; sodium hydroxide; lithium aluminium tetrahydride; aluminium trichloride; oxalyl dichloride; potassium tert-butylate; oxalic acid; lithium; In tetrahydrofuran; methanol; diethyl ether; ammonia; water; ethylene glycol; dimethyl sulfoxide; benzene;