N,N-bis(2E,7-octadienyl)aniline

Base Information

Chemical Name:N,N-bis(2E,7-octadienyl)aniline
CAS No.:81051-01-6
Molecular Formula:C₂₂H₃₁N
Molecular Weight:309.495
Hs Code.:

Synonyms:N,N-bis(2E,7-octadienyl)aniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-bis(2E,7-octadienyl)aniline

Chemical Property:

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Technology Process of N,N-bis(2E,7-octadienyl)aniline

There total 4 articles about N,N-bis(2E,7-octadienyl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106-99-0,130983-70-9,29406-96-0,9003-17-2
buta-1,3-diene

: 62-53-3
aniline

: 35755-82-9
(E)-N-(octa-2,7-dien-1-yl)aniline

: 81051-01-6
N,N-bis(2E,7-octadienyl)aniline

Guidance literature:: palladium(II) acetylacetonate; triethylaluminum; triphenylphosphine; In benzene; at 100 ℃; Product distribution; reaction in the presence of CF₃CO₂H; telomerization of anilines with butadiene in the presence of Pd complexes, influence of basicity and substituent position in aniline on the direction and selectivity of telomerization;
DOI:10.1007/BF00951898

Reference yield:

: 139571-92-9
Diethyl-methyl-((E)-octa-2,7-dienyl)-ammonium; iodide

: 81051-01-6
N,N-bis(2E,7-octadienyl)aniline

Guidance literature:: Multi-step reaction with 2 steps

1: 1) i-Bu₃Al / 2) Pd(Ph₃P)2Cl₂ / 1) CH₂Cl₂, 40 deg C, 1 h, 2) 40 deg C, 8 h

2: 1) i-Bu₂AlCl / 2) Pd(acac)2 + 2Ph₃P / 1) CH₂Cl₂, 40 deg C, 1 h, 2) 40 deg C, 8 h

With triisobutylaluminum; diisobutylaluminum chloride; bis-triphenylphosphine-palladium(II) chloride; palladium(II) acetylacetonate; triphenylphosphine;
DOI:10.1007/BF00957997

Reference yield:

: 62-53-3
aniline

: 81051-01-6
N,N-bis(2E,7-octadienyl)aniline

Guidance literature:: Multi-step reaction with 2 steps

1: 1) i-Bu₃Al / 2) Pd(Ph₃P)2Cl₂ / 1) CH₂Cl₂, 40 deg C, 1 h, 2) 40 deg C, 8 h

2: 1) i-Bu₂AlCl / 2) Pd(acac)2 + 2Ph₃P / 1) CH₂Cl₂, 40 deg C, 1 h, 2) 40 deg C, 8 h

With triisobutylaluminum; diisobutylaluminum chloride; bis-triphenylphosphine-palladium(II) chloride; palladium(II) acetylacetonate; triphenylphosphine;
DOI:10.1007/BF00957997