Technology Process of C23H34N2O3
There total 5 articles about C23H34N2O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Ethyl oxalyl chloride; 2-(3-methoxyphenyl)-1-ethanamine;
With
triethylamine;
In
dichloromethane;
at 0 ℃;
for 1h;
screw cap vial;
(2E,4E)-dodeca-2,4-dien-1-amine;
In
ethanol;
at 60 ℃;
for 15h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: diphenylphosphoranyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene
2.1: lithium aluminium tetrahydride / diethyl ether / 2 h / 0 - 20 °C / Inert atmosphere; Cooling with ice
3.1: triethylamine / dichloromethane / 1 h / 0 °C / screw cap vial
3.2: 15 h / 60 °C
With
lithium aluminium tetrahydride; diphenylphosphoranyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine;
In
diethyl ether; dichloromethane; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: diisobutylaluminium hydride / n-heptane; hexane / 0.75 h / -70 °C / Inert atmosphere
2.1: diphenylphosphoranyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene
3.1: lithium aluminium tetrahydride / diethyl ether / 2 h / 0 - 20 °C / Inert atmosphere; Cooling with ice
4.1: triethylamine / dichloromethane / 1 h / 0 °C / screw cap vial
4.2: 15 h / 60 °C
With
lithium aluminium tetrahydride; diphenylphosphoranyl azide; diisobutylaluminium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine;
In
diethyl ether; hexane; n-heptane; dichloromethane; toluene;
