10b-(4-chlorophenyl)-11-methylene-10b,11-dihydro-6H-isoindolo[2,1-a]indol-6-one

Base Information

Chemical Name:10b-(4-chlorophenyl)-11-methylene-10b,11-dihydro-6H-isoindolo[2,1-a]indol-6-one
CAS No.:1370410-58-4
Molecular Formula:C₂₂H₁₄ClNO
Molecular Weight:343.812
Hs Code.:

Synonyms:10b-(4-chlorophenyl)-11-methylene-10b,11-dihydro-6H-isoindolo[2,1-a]indol-6-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 10b-(4-chlorophenyl)-11-methylene-10b,11-dihydro-6H-isoindolo[2,1-a]indol-6-one

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Technology Process of 10b-(4-chlorophenyl)-11-methylene-10b,11-dihydro-6H-isoindolo[2,1-a]indol-6-one

There total 2 articles about 10b-(4-chlorophenyl)-11-methylene-10b,11-dihydro-6H-isoindolo[2,1-a]indol-6-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1370410-27-7
C₂₂H₁₅ClINO

: 1370410-58-4
10b-(4-chlorophenyl)-11-methylene-10b,11-dihydro-6H-isoindolo[2,1-a]indol-6-one

Guidance literature:: With sodium phosphate dibasic dodecahydrate; silver(I) acetate; palladium diacetate; In N,N-dimethyl-formamide; at 80 ℃; for 12h;
DOI:10.1021/ol300584m

Reference yield: 77.0%

: 2809-65-6
4-chloro-1-propynylbenzene

: 202132-25-0
2-bromo-N-(2-iodophenyl)benzamide

: 1370410-58-4
10b-(4-chlorophenyl)-11-methylene-10b,11-dihydro-6H-isoindolo[2,1-a]indol-6-one

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; triethylamine; lithium chloride; In N,N-dimethyl-formamide; at 120 ℃; Schlenk technique; Inert atmosphere;
DOI:10.1039/c9cc03566d