C₅₉H₆₉NO₁₅Si

Base Information

Chemical Name:C₅₉H₆₉NO₁₅Si
CAS No.:260249-52-3
Molecular Formula:C₅₉H₆₉NO₁₅Si
Molecular Weight:1060.28
Hs Code.:

C<sub>59</sub>H<sub>69</sub>NO<sub>15</sub>Si

Synonyms:C₅₉H₆₉NO₁₅Si

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Chemical Property of C₅₉H₆₉NO₁₅Si

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Technology Process of C₅₉H₆₉NO₁₅Si

There total 5 articles about C₅₉H₆₉NO₁₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 260249-52-3
C₅₉H₆₉NO₁₅Si

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / pyridine / 3 h / 20 °C

2: TsN₃; Et₃N; DBU / acetonitrile / 16 h / 20 °C

3: 80 percent / Cu(acac)2 / 70 h / 60 °C

4: ([Bu]2Sn(Cl))2O / ethanol / 24 h / Heating

With copper acetylacetonate; 4-toluenesulfonyl azide; 1,3-dichlorotetrabutyldistannoxane; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In pyridine; ethanol; acetonitrile; 1: Condensation / 2: Diazotization / 3: Substitution / 4: transesterification;
DOI:10.1016/S0040-4039(99)02056-0

Reference yield:

: 260245-86-1
C₅₂H₆₂O₁₄Si

: 260249-52-3
C₅₉H₆₉NO₁₅Si

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / pyridine / 3 h / 20 °C

2: TsN₃; Et₃N; DBU / acetonitrile / 16 h / 20 °C

3: 80 percent / Cu(acac)2 / 70 h / 60 °C

4: ([Bu]2Sn(Cl))2O / ethanol / 24 h / Heating

With copper acetylacetonate; 4-toluenesulfonyl azide; 1,3-dichlorotetrabutyldistannoxane; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In pyridine; ethanol; acetonitrile; 1: Condensation / 2: Diazotization / 3: Substitution / 4: transesterification;
DOI:10.1016/S0040-4039(99)02056-0

Reference yield:

: 260249-46-5
C₅₉H₆₉NO₁₄Si

: 260249-52-3
C₅₉H₆₉NO₁₅Si

Guidance literature:: Multi-step reaction with 3 steps

1: TsN₃; Et₃N; DBU / acetonitrile / 16 h / 20 °C

2: 80 percent / Cu(acac)2 / 70 h / 60 °C

3: ([Bu]2Sn(Cl))2O / ethanol / 24 h / Heating

With copper acetylacetonate; 4-toluenesulfonyl azide; 1,3-dichlorotetrabutyldistannoxane; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In ethanol; acetonitrile; 1: Diazotization / 2: Substitution / 3: transesterification;
DOI:10.1016/S0040-4039(99)02056-0