3-[5'-fluoro-2'-methoxy-(1,1'-biphenyl)-3-yl][1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6-thiol

Base Information

Chemical Name:3-[5'-fluoro-2'-methoxy-(1,1'-biphenyl)-3-yl][1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6-thiol
CAS No.:1560987-49-6
Molecular Formula:C₁₆H₁₁FN₄OS₂
Molecular Weight:358.42
Hs Code.:

Synonyms:3-[5'-fluoro-2'-methoxy-(1,1'-biphenyl)-3-yl][1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6-thiol

Suppliers and Price of 3-[5'-fluoro-2'-methoxy-(1,1'-biphenyl)-3-yl][1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6-thiol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-[5'-fluoro-2'-methoxy-(1,1'-biphenyl)-3-yl][1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6-thiol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-[5'-fluoro-2'-methoxy-(1,1'-biphenyl)-3-yl][1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6-thiol

There total 2 articles about 3-[5'-fluoro-2'-methoxy-(1,1'-biphenyl)-3-yl][1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6-thiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 75-15-0,12122-00-8
carbon disulfide

: 1401008-58-9
4-amino-5-[5'-fluoro-2'-methoxy-(1,1'-biphenyl)-3-yl]-4H-1,2,4-triazole-3-thiol

: 1560987-49-6
3-[5'-fluoro-2'-methoxy-(1,1'-biphenyl)-3-yl][1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6-thiol

Guidance literature:: With potassium hydroxide; In ethanol; for 4h; Reflux;
DOI:10.1007/s00044-014-0944-x

Reference yield:

: 1253043-52-5
C₁₅H₁₁FN₂O₂S

: 1560987-49-6
3-[5'-fluoro-2'-methoxy-(1,1'-biphenyl)-3-yl][1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6-thiol

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / 6 h / Reflux

2: potassium hydroxide / ethanol / 4 h / Reflux

With hydrazine hydrate; potassium hydroxide; In ethanol;
DOI:10.1007/s00044-014-0944-x

Reference yield: 85.0%

: 1560987-49-6
3-[5'-fluoro-2'-methoxy-(1,1'-biphenyl)-3-yl][1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6-thiol

: 5332-06-9
4-bromobutanenitrile

: 1560987-63-4
4-{[3-(5'-fluoro-2'-methoxy-(1,1'-biphenyl)-3-yl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-6-yl]sulfanyl}butanenitrile

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 0.0833333h; Temperature; Microwave irradiation;
DOI:10.1007/s00044-014-0944-x