4-amino-5-[5'-fluoro-2'-methoxy-(1,1'-biphenyl)-3-yl]-4H-1,2,4-triazole-3-thiol

Base Information

Chemical Name:4-amino-5-[5'-fluoro-2'-methoxy-(1,1'-biphenyl)-3-yl]-4H-1,2,4-triazole-3-thiol
CAS No.:1401008-58-9
Molecular Formula:C₁₅H₁₃FN₄OS
Molecular Weight:316.359
Hs Code.:

Synonyms:4-amino-5-[5'-fluoro-2'-methoxy-(1,1'-biphenyl)-3-yl]-4H-1,2,4-triazole-3-thiol

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Chemical Property of 4-amino-5-[5'-fluoro-2'-methoxy-(1,1'-biphenyl)-3-yl]-4H-1,2,4-triazole-3-thiol

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Technology Process of 4-amino-5-[5'-fluoro-2'-methoxy-(1,1'-biphenyl)-3-yl]-4H-1,2,4-triazole-3-thiol

There total 1 articles about 4-amino-5-[5'-fluoro-2'-methoxy-(1,1'-biphenyl)-3-yl]-4H-1,2,4-triazole-3-thiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1253043-52-5
C₁₅H₁₁FN₂O₂S

: 1401008-58-9
4-amino-5-[5'-fluoro-2'-methoxy-(1,1'-biphenyl)-3-yl]-4H-1,2,4-triazole-3-thiol

Guidance literature:: With hydrazine hydrate; In ethanol; for 6h; Reflux;
DOI:10.1007/s00044-014-0944-x

Reference yield: 89.0%

: 75-15-0,12122-00-8
carbon disulfide

: 1401008-58-9
4-amino-5-[5'-fluoro-2'-methoxy-(1,1'-biphenyl)-3-yl]-4H-1,2,4-triazole-3-thiol

: 1560987-49-6
3-[5'-fluoro-2'-methoxy-(1,1'-biphenyl)-3-yl][1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6-thiol

Guidance literature:: With potassium hydroxide; In ethanol; for 4h; Reflux;
DOI:10.1007/s00044-014-0944-x

Reference yield:

: 1401008-58-9
4-amino-5-[5'-fluoro-2'-methoxy-(1,1'-biphenyl)-3-yl]-4H-1,2,4-triazole-3-thiol

: C₂₇H₂₀FN₅O₃S₂

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / ethanol / 4 h / Reflux

2: potassium carbonate / N,N-dimethyl-formamide / 0.08 h / 50 °C / Microwave irradiation

With potassium carbonate; potassium hydroxide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1007/s00044-014-0944-x