2-azido-3-O-benzyl-2-deoxy-4,6-O-(2-naphthylmethylidene)-β-D-glucopyranosyl benzoate

Base Information

Chemical Name:2-azido-3-O-benzyl-2-deoxy-4,6-O-(2-naphthylmethylidene)-β-D-glucopyranosyl benzoate
CAS No.:657394-99-5
Molecular Formula:C₃₁H₂₇N₃O₆
Molecular Weight:537.572
Hs Code.:

Synonyms:2-azido-3-O-benzyl-2-deoxy-4,6-O-(2-naphthylmethylidene)-β-D-glucopyranosyl benzoate

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Chemical Property of 2-azido-3-O-benzyl-2-deoxy-4,6-O-(2-naphthylmethylidene)-β-D-glucopyranosyl benzoate

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Technology Process of 2-azido-3-O-benzyl-2-deoxy-4,6-O-(2-naphthylmethylidene)-β-D-glucopyranosyl benzoate

There total 8 articles about 2-azido-3-O-benzyl-2-deoxy-4,6-O-(2-naphthylmethylidene)-β-D-glucopyranosyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 100-39-0
benzyl bromide

: 923952-61-8
2-azido-2-deoxy-4,6-O-(2-naphthylmethylidene)-β-D-glucopyranosyl benzoate

: 657394-99-5
2-azido-3-O-benzyl-2-deoxy-4,6-O-(2-naphthylmethylidene)-β-D-glucopyranosyl benzoate

Guidance literature:: With silver(l) oxide; In dichloromethane; at 20 ℃; for 48h;
DOI:10.1021/ol062464t

Reference yield:

: (2R,4aR,7R,8R,8aS)-7-Azido-2-naphthalen-2-yl-hexahydro-pyrano[3,2-d][1,3]dioxine-6,8-diol

: 657394-99-5
2-azido-3-O-benzyl-2-deoxy-4,6-O-(2-naphthylmethylidene)-β-D-glucopyranosyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / triethylamine / CH₂Cl₂ / cooling

2: 83 percent / silver(I) oxide / CH₂Cl₂ / 48 h / 20 °C

With triethylamine; silver(l) oxide; In dichloromethane;
DOI:10.1021/ol062464t

Reference yield:

: 93-97-0
benzoic acid anhydride

: 657394-99-5
2-azido-3-O-benzyl-2-deoxy-4,6-O-(2-naphthylmethylidene)-β-D-glucopyranosyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / triethylamine / CH₂Cl₂ / cooling

2: 83 percent / silver(I) oxide / CH₂Cl₂ / 48 h / 20 °C

With triethylamine; silver(l) oxide; In dichloromethane;
DOI:10.1021/ol062464t