8-acetamido-4-[N-(4-acetamidophenyl)-N-methylamino]-2-methylpyrazolo[1,5-a]-1,3,5-triazine

Base Information

Chemical Name:8-acetamido-4-[N-(4-acetamidophenyl)-N-methylamino]-2-methylpyrazolo[1,5-a]-1,3,5-triazine
CAS No.:652539-00-9
Molecular Formula:C₁₇H₁₉N₇O₂
Molecular Weight:353.384
Hs Code.:

Synonyms:8-acetamido-4-[N-(4-acetamidophenyl)-N-methylamino]-2-methylpyrazolo[1,5-a]-1,3,5-triazine

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Chemical Property of 8-acetamido-4-[N-(4-acetamidophenyl)-N-methylamino]-2-methylpyrazolo[1,5-a]-1,3,5-triazine

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Technology Process of 8-acetamido-4-[N-(4-acetamidophenyl)-N-methylamino]-2-methylpyrazolo[1,5-a]-1,3,5-triazine

There total 3 articles about 8-acetamido-4-[N-(4-acetamidophenyl)-N-methylamino]-2-methylpyrazolo[1,5-a]-1,3,5-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 75-36-5
acetyl chloride

: 527704-23-0
8-amino-4-[N-(4-aminophenyl)-N-methylamino]pyrazolo[1,5-a]-1,3,5-triazine

: 652539-00-9
8-acetamido-4-[N-(4-acetamidophenyl)-N-methylamino]-2-methylpyrazolo[1,5-a]-1,3,5-triazine

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 476468-38-9
2-methyl-4-(N-methyl-N-phenylamino)pyrazolo[1,5-a]-1,3,5-triazin-4-one

: 652539-00-9
8-acetamido-4-[N-(4-acetamidophenyl)-N-methylamino]-2-methylpyrazolo[1,5-a]-1,3,5-triazine

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / fuming nitric acid / 0.17 h / 0 °C

2: 68 percent / H₂ / Pd/C / methanol / 2 h / 20 °C

3: triethylamine / CH₂Cl₂ / 0.08 h / 0 - 20 °C

With hydrogen; nitric acid; triethylamine; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1016/S0040-4039(02)02661-8

Reference yield:

: 527704-22-9
2-methyl-4-[N-methyl-N-(4-nitrophenyl)amino]-8-nitropyrazolo[1,5-a]-1,3,5-triazine

: 652539-00-9
8-acetamido-4-[N-(4-acetamidophenyl)-N-methylamino]-2-methylpyrazolo[1,5-a]-1,3,5-triazine

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / H₂ / Pd/C / methanol / 2 h / 20 °C

2: triethylamine / CH₂Cl₂ / 0.08 h / 0 - 20 °C

With hydrogen; triethylamine; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1016/S0040-4039(02)02661-8