(S)-4-benzyl-3-[4-(tert-butyldimethylsilanyloxy)butanoyl]oxazolidin-2-one

Base Information

Chemical Name:(S)-4-benzyl-3-[4-(tert-butyldimethylsilanyloxy)butanoyl]oxazolidin-2-one
CAS No.:936731-49-6
Molecular Formula:C₂₀H₃₁NO₄Si
Molecular Weight:377.556
Hs Code.:

Synonyms:(S)-4-benzyl-3-[4-(tert-butyldimethylsilanyloxy)butanoyl]oxazolidin-2-one

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Chemical Property of (S)-4-benzyl-3-[4-(tert-butyldimethylsilanyloxy)butanoyl]oxazolidin-2-one

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Technology Process of (S)-4-benzyl-3-[4-(tert-butyldimethylsilanyloxy)butanoyl]oxazolidin-2-one

There total 5 articles about (S)-4-benzyl-3-[4-(tert-butyldimethylsilanyloxy)butanoyl]oxazolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 69171-62-6
4-(tert-butyl(dimethyl)silanyloxy)butyric acid

: 90719-32-7
(S)-4-Benzyl-2-oxazolidinone

: 936731-49-6
(S)-4-benzyl-3-[4-(tert-butyldimethylsilanyloxy)butanoyl]oxazolidin-2-one

Guidance literature:: 4-(tert-butyl(dimethyl)silanyloxy)butyric acid; With pivaloyl chloride; triethylamine; In tetrahydrofuran; at -78 ℃; for 1h;

(S)-4-Benzyl-2-oxazolidinone; With lithium chloride; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1002/asia.201700555

Reference yield: 74.0%

: 69171-62-6
4-(tert-butyl(dimethyl)silanyloxy)butyric acid

: 101711-90-4,123731-35-1,128677-61-2
(S)-4-benzyl-2-oxazolidinone lithium salt

: 936731-49-6
(S)-4-benzyl-3-[4-(tert-butyldimethylsilanyloxy)butanoyl]oxazolidin-2-one

Guidance literature:: 4-(tert-butyl(dimethyl)silanyloxy)butyric acid; With chloroformic acid ethyl ester; In tetrahydrofuran; at -78 - 0 ℃; for 1h;

(S)-4-benzyl-2-oxazolidinone lithium salt; In tetrahydrofuran;
DOI:10.1016/j.tetlet.2011.05.107

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 169897-87-4
[4S]-4-benzyl-3-(4-benzyloxy-1-butanoyl)-2-oxazolidinone

: 936731-49-6
(S)-4-benzyl-3-[4-(tert-butyldimethylsilanyloxy)butanoyl]oxazolidin-2-one

Guidance literature:: [4S]-4-benzyl-3-(4-benzyloxy-1-butanoyl)-2-oxazolidinone; With hydrogen; palladium hydroxide on carbon; In ethanol; for 24h;

tert-butyldimethylsilyl chloride; With 1H-imidazole; In tetrahydrofuran; at 0 - 20 ℃; for 4h;