ethyl (4-{3-[(4-fluorophenyl)sulphonyl]-4-hydroxybenzyl}-3,5-dimethylphenoxy)acetate

Base Information

Chemical Name:ethyl (4-{3-[(4-fluorophenyl)sulphonyl]-4-hydroxybenzyl}-3,5-dimethylphenoxy)acetate
CAS No.:459431-01-7
Molecular Formula:C₂₅H₂₅FO₆S
Molecular Weight:472.534
Hs Code.:

Synonyms:ethyl (4-{3-[(4-fluorophenyl)sulphonyl]-4-hydroxybenzyl}-3,5-dimethylphenoxy)acetate

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Chemical Property of ethyl (4-{3-[(4-fluorophenyl)sulphonyl]-4-hydroxybenzyl}-3,5-dimethylphenoxy)acetate

Chemical Property:

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Technology Process of ethyl (4-{3-[(4-fluorophenyl)sulphonyl]-4-hydroxybenzyl}-3,5-dimethylphenoxy)acetate

There total 14 articles about ethyl (4-{3-[(4-fluorophenyl)sulphonyl]-4-hydroxybenzyl}-3,5-dimethylphenoxy)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 459430-99-0
ethyl (4-{4-(benzyloxy)-3-[(4-fluorophenyl)sulphonyl]benzyl}-3,5-dimethylphenoxy)acetate

: 459431-01-7
ethyl (4-{3-[(4-fluorophenyl)sulphonyl]-4-hydroxybenzyl}-3,5-dimethylphenoxy)acetate

Guidance literature:: palladium on activated carbon; In ethanol;

Reference yield:

: 459430-90-1
[4-(benzyloxy)-3-bromophenyl]methanol

: 459431-01-7
ethyl (4-{3-[(4-fluorophenyl)sulphonyl]-4-hydroxybenzyl}-3,5-dimethylphenoxy)acetate

Guidance literature:: Multi-step reaction with 10 steps

1: water; N,N-dimethyl-formamide

2: ammonium chloride; tert.-butyl lithium / tetrahydrofuran; hexane

3: dichloromethane; ethyl acetate

4: tetra-n-butylammoniumfluoride trihydrate / tetrahydrofuran; ethyl acetate

5: dichloromethane

6: n-butyllithium; ammonium chloride / tetrahydrofuran; hexane

7: triethylsilane; ammonium chloride / tetrahydrofuran

8: tetrabutyl ammonium fluoride / 1,1-dichloroethane; ethyl acetate

9: ammonium chloride; potassium carbonate / N-methyl-acetamide

10: palladium on activated carbon / ethanol

With triethylsilane; n-butyllithium; ammonium chloride; tetrabutyl ammonium fluoride; tert.-butyl lithium; potassium carbonate; tetra-n-butylammoniumfluoride trihydrate; palladium on activated carbon; In tetrahydrofuran; N-methyl-acetamide; 1,1-dichloroethane; ethanol; hexane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 459430-93-4
({4-(benzyloxy)-3-[(4-fluorophenyl)sulphonyl]benzyl}oxy)(tert-butyl)dimethylsilane

: 459431-01-7
ethyl (4-{3-[(4-fluorophenyl)sulphonyl]-4-hydroxybenzyl}-3,5-dimethylphenoxy)acetate

Guidance literature:: Multi-step reaction with 7 steps

1: tetra-n-butylammoniumfluoride trihydrate / tetrahydrofuran; ethyl acetate

2: dichloromethane

3: n-butyllithium; ammonium chloride / tetrahydrofuran; hexane

4: triethylsilane; ammonium chloride / tetrahydrofuran

5: tetrabutyl ammonium fluoride / 1,1-dichloroethane; ethyl acetate

6: ammonium chloride; potassium carbonate / N-methyl-acetamide

7: palladium on activated carbon / ethanol

With triethylsilane; n-butyllithium; ammonium chloride; tetrabutyl ammonium fluoride; potassium carbonate; tetra-n-butylammoniumfluoride trihydrate; palladium on activated carbon; In tetrahydrofuran; N-methyl-acetamide; 1,1-dichloroethane; ethanol; hexane; dichloromethane; ethyl acetate;