ethyl (4-{4-(benzyloxy)-3-[(4-fluorophenyl)sulphonyl]benzyl}-3,5-dimethylphenoxy)acetate

Base Information

Chemical Name:ethyl (4-{4-(benzyloxy)-3-[(4-fluorophenyl)sulphonyl]benzyl}-3,5-dimethylphenoxy)acetate
CAS No.:459430-99-0
Molecular Formula:C₃₂H₃₁FO₆S
Molecular Weight:562.659
Hs Code.:

Synonyms:ethyl (4-{4-(benzyloxy)-3-[(4-fluorophenyl)sulphonyl]benzyl}-3,5-dimethylphenoxy)acetate

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Chemical Property of ethyl (4-{4-(benzyloxy)-3-[(4-fluorophenyl)sulphonyl]benzyl}-3,5-dimethylphenoxy)acetate

Chemical Property:

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Technology Process of ethyl (4-{4-(benzyloxy)-3-[(4-fluorophenyl)sulphonyl]benzyl}-3,5-dimethylphenoxy)acetate

There total 12 articles about ethyl (4-{4-(benzyloxy)-3-[(4-fluorophenyl)sulphonyl]benzyl}-3,5-dimethylphenoxy)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 459430-98-9
4-{4-(benzyloxy)-3-[(4-fluorophenyl)sulphonyl]benzyl}-3,5-dimethylphenol

: 40258-78-4
1-bromoethyl acetate

: 459430-99-0
ethyl (4-{4-(benzyloxy)-3-[(4-fluorophenyl)sulphonyl]benzyl}-3,5-dimethylphenoxy)acetate

Guidance literature:: With ammonium chloride; potassium carbonate; In N-methyl-acetamide;

Reference yield:

: 459430-91-2
{[4-(benzyloxy)-3-bromobenzyl]oxy}(tert-butyl)dimethylsilane

: 459430-99-0
ethyl (4-{4-(benzyloxy)-3-[(4-fluorophenyl)sulphonyl]benzyl}-3,5-dimethylphenoxy)acetate

Guidance literature:: Multi-step reaction with 8 steps

1: ammonium chloride; tert.-butyl lithium / tetrahydrofuran; hexane

2: dichloromethane; ethyl acetate

3: tetra-n-butylammoniumfluoride trihydrate / tetrahydrofuran; ethyl acetate

4: dichloromethane

5: n-butyllithium; ammonium chloride / tetrahydrofuran; hexane

6: triethylsilane; ammonium chloride / tetrahydrofuran

7: tetrabutyl ammonium fluoride / 1,1-dichloroethane; ethyl acetate

8: ammonium chloride; potassium carbonate / N-methyl-acetamide

With triethylsilane; n-butyllithium; ammonium chloride; tetrabutyl ammonium fluoride; tert.-butyl lithium; potassium carbonate; tetra-n-butylammoniumfluoride trihydrate; In tetrahydrofuran; N-methyl-acetamide; 1,1-dichloroethane; hexane; dichloromethane; ethyl acetate;

Reference yield:

: 459430-95-6
4-(benzyloxy)-3-[(4-fluorophenyl)sulphonyl]benzaldehyde

: 459430-99-0
ethyl (4-{4-(benzyloxy)-3-[(4-fluorophenyl)sulphonyl]benzyl}-3,5-dimethylphenoxy)acetate

Guidance literature:: Multi-step reaction with 4 steps

1: n-butyllithium; ammonium chloride / tetrahydrofuran; hexane

2: triethylsilane; ammonium chloride / tetrahydrofuran

3: tetrabutyl ammonium fluoride / 1,1-dichloroethane; ethyl acetate

4: ammonium chloride; potassium carbonate / N-methyl-acetamide

With triethylsilane; n-butyllithium; ammonium chloride; tetrabutyl ammonium fluoride; potassium carbonate; In tetrahydrofuran; N-methyl-acetamide; 1,1-dichloroethane; hexane; ethyl acetate;