(1R,2R)-2-chlorocyclohexanol

Base Information Edit

Chemical Name:(1R,2R)-2-chlorocyclohexanol
CAS No.:931-13-5
Molecular Formula:C₆H₁₁ClO
Molecular Weight:134.606
Hs Code.:
Mol file:931-13-5.mol

Synonyms:(1R,2R)-2-chlorocyclohexanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2R)-2-chlorocyclohexanol Edit

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Technology Process of (1R,2R)-2-chlorocyclohexanol

There total 20 articles about (1R,2R)-2-chlorocyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 286-20-4
cyclohexene oxide

: 85116-37-6
(-)-diisopinocamphenylborane chloride

: (C₁₀H₁₇)BNH(C₂H₄O)2

: 931-13-5
(1R,2R)-2-chlorocyclohexanol

Guidance literature:: With butyraldehyde; 2,2'-iminobis[ethanol]; In pentane; cooling of a pentane soln. of 1.0 M borane to -100°C (under N2), dropwise addn. of epoxide in pentane, addn. of butyraldehyde, warming to room temp., diluting with pentane and then addn. of diethanolamine; monitored bei (11)B NMR, filtn. of B-complex, washing of the filtrate with water, drying with anhyd. Na2SO4, concn. in vac., flash chromy. on silica gel (ether/hexane), distn. of halohydrine, 22 % ee;