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(1R,2R)-2-chlorocyclohexanol

Base Information Edit
  • Chemical Name:(1R,2R)-2-chlorocyclohexanol
  • CAS No.:931-13-5
  • Molecular Formula:C6H11ClO
  • Molecular Weight:134.606
  • Hs Code.:
  • Mol file:931-13-5.mol
(1R,2R)-2-chlorocyclohexanol

Synonyms:(1R,2R)-2-chlorocyclohexanol

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Chemical Property of (1R,2R)-2-chlorocyclohexanol Edit
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Technology Process of (1R,2R)-2-chlorocyclohexanol

There total 20 articles about (1R,2R)-2-chlorocyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With butyraldehyde; 2,2'-iminobis[ethanol]; In pentane; cooling of a pentane soln. of 1.0 M borane to -100°C (under N2), dropwise addn. of epoxide in pentane, addn. of butyraldehyde, warming to room temp., diluting with pentane and then addn. of diethanolamine; monitored bei (11)B NMR, filtn. of B-complex, washing of the filtrate with water, drying with anhyd. Na2SO4, concn. in vac., flash chromy. on silica gel (ether/hexane), distn. of halohydrine, 22 % ee;
Guidance literature:
With methanol; potassium carbonate; at 20 ℃;
DOI:10.1016/j.tetasy.2012.11.011
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