2-chlorocyclohexylbutyrate

Base Information

• Chemical Name: 2-chlorocyclohexylbutyrate
• CAS No.: 134070-91-0
• Molecular Formula: C₁₀H₁₇ClO₂
• Molecular Weight: 204.697

Synonyms:

Chemical Property of 2-chlorocyclohexylbutyrate

Chemical Property:

Purity/Quality:

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Technology Process of 2-chlorocyclohexylbutyrate

There total 3 articles about 2-chlorocyclohexylbutyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

butanoic acid anhydride (106-31-0) + trans-2-chlorocyclohexanol (6628-80-4) → 2-chlorocyclohexylbutyrate (134070-91-0,134108-82-0,134733-51-0)

Guidance literature:

With pyridine; dmap; In dichloromethane; for 2h; Ambient temperature;

Reference yield: 86.0%

cyclohexane-1,2-epoxide (286-20-4) + butyryl chloride (141-75-3) → 2-chlorocyclohexylbutyrate (134070-91-0,134108-82-0,134733-51-0)

Guidance literature:

With tris(dipivaloylmethanato)europium(III); In benzene; at 40 ℃; for 4h;

DOI:10.1016/S0040-4039(98)00831-4

Reference yield: 79.0%

cyclohexane-1,2-epoxide (286-20-4) + butyryl chloride (141-75-3) → octane-4,5-dione (5455-24-3) + 2-chlorocyclohexylbutyrate (134070-91-0,134108-82-0,134733-51-0)

Guidance literature:

CoCl₂; In acetonitrile; Yields of byproduct given; Ambient temperature;

DOI:10.1016/S0040-4020(01)96041-7

upstream raw materials:

butanoic acid anhydride

trans-2-chlorocyclohexanol

cyclohexane-1,2-epoxide

butyryl chloride

Downstream raw materials:

(1R,2R)-2-chlorocyclohexanol

Butyric acid (1S,2S)-2-chloro-cyclohexyl ester

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