methyl {3-[(S)-2-((S)-1-phenylethylamino)propyl]phenyl}acetate hydrochloride

Base Information

Chemical Name:methyl {3-[(S)-2-((S)-1-phenylethylamino)propyl]phenyl}acetate hydrochloride
CAS No.:1253582-12-5
Molecular Formula:C₂₀H₂₅NO₂*ClH
Molecular Weight:347.885
Hs Code.:

Synonyms:methyl {3-[(S)-2-((S)-1-phenylethylamino)propyl]phenyl}acetate hydrochloride

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Chemical Property of methyl {3-[(S)-2-((S)-1-phenylethylamino)propyl]phenyl}acetate hydrochloride

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Technology Process of methyl {3-[(S)-2-((S)-1-phenylethylamino)propyl]phenyl}acetate hydrochloride

There total 3 articles about methyl {3-[(S)-2-((S)-1-phenylethylamino)propyl]phenyl}acetate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 792917-99-8
methyl [3-(2-oxopropyl)phenyl]acetate

: 2627-86-3
(S)-1-phenyl-ethylamine

: 1253582-12-5
methyl {3-[(S)-2-((S)-1-phenylethylamino)propyl]phenyl}acetate hydrochloride

Guidance literature:: methyl [3-(2-oxopropyl)phenyl]acetate; (S)-1-phenyl-ethylamine; With sodium tris(acetoxy)borohydride; magnesium sulfate; In dichloromethane;

With sodium hydrogencarbonate; In dichloromethane; water; at 0 ℃;

With hydrogenchloride; In water;

Reference yield:

: 1878-67-7
3-Bromophenylacetic acid

: 1253582-12-5
methyl {3-[(S)-2-((S)-1-phenylethylamino)propyl]phenyl}acetate hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid / 16 h / 40 °C

2.1: tributyltin methoxide / palladium diacetate; tris-(o-tolyl)phosphine / toluene / 6 h / 100 °C

3.1: sodium tris(acetoxy)borohydride; magnesium sulfate / dichloromethane

3.2: 0 °C

With sulfuric acid; tributyltin methoxide; sodium tris(acetoxy)borohydride; magnesium sulfate; palladium diacetate; tris-(o-tolyl)phosphine; In dichloromethane; toluene;

Reference yield:

: 150529-73-0
methyl 2-(3-bromophenyl)acetatee

: 1253582-12-5
methyl {3-[(S)-2-((S)-1-phenylethylamino)propyl]phenyl}acetate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: tributyltin methoxide / palladium diacetate; tris-(o-tolyl)phosphine / toluene / 6 h / 100 °C

2.1: sodium tris(acetoxy)borohydride; magnesium sulfate / dichloromethane

2.2: 0 °C

With tributyltin methoxide; sodium tris(acetoxy)borohydride; magnesium sulfate; palladium diacetate; tris-(o-tolyl)phosphine; In dichloromethane; toluene;