6-(4-methoxyphenyl)-2-[6-(4-methylpiperazin-1-yl)pyridin-3-yl]-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene hydrochloride

Base Information

Chemical Name:6-(4-methoxyphenyl)-2-[6-(4-methylpiperazin-1-yl)pyridin-3-yl]-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene hydrochloride
CAS No.:1469858-78-3
Molecular Formula:C₂₅H₂₅N₅OS*ClH
Molecular Weight:480.033
Hs Code.:

Synonyms:6-(4-methoxyphenyl)-2-[6-(4-methylpiperazin-1-yl)pyridin-3-yl]-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene hydrochloride

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Chemical Property of 6-(4-methoxyphenyl)-2-[6-(4-methylpiperazin-1-yl)pyridin-3-yl]-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene hydrochloride

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Technology Process of 6-(4-methoxyphenyl)-2-[6-(4-methylpiperazin-1-yl)pyridin-3-yl]-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene hydrochloride

There total 7 articles about 6-(4-methoxyphenyl)-2-[6-(4-methylpiperazin-1-yl)pyridin-3-yl]-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1469858-60-3
6-(4-methoxyphenyl)-2-[6-(4-methylpiperazin-1-yl)pyridin-3-yl]-4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

: 1469858-78-3
6-(4-methoxyphenyl)-2-[6-(4-methylpiperazin-1-yl)pyridin-3-yl]-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene hydrochloride

Guidance literature:: With hydrogenchloride; In methanol; at 100 ℃; for 4h;

Reference yield:

: 1469857-45-1
2-bromo-6-(4-methoxyphenyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

: 1469858-78-3
6-(4-methoxyphenyl)-2-[6-(4-methylpiperazin-1-yl)pyridin-3-yl]-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 80 °C

2: sodium carbonate; bis-triphenylphosphine-palladium(II) chloride / ethanol; toluene / 8 h / 100 °C

3: hydrogenchloride / methanol / 4 h / 100 °C

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; sodium hydride; sodium carbonate; In tetrahydrofuran; methanol; ethanol; toluene; mineral oil;

Reference yield:

: 4181-97-9
phenyl 4-methoxybenzoate

: 1469858-78-3
6-(4-methoxyphenyl)-2-[6-(4-methylpiperazin-1-yl)pyridin-3-yl]-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene hydrochloride

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydride / tetrahydrofuran; mineral oil / 8 h / 100 °C

2: hydrazine hydrate; acetic acid / ethanol / 4 h / 100 °C / Inert atmosphere

3: acetic acid; bromine / 12 h / 80 °C

4: sodium hydride / tetrahydrofuran; mineral oil / 0 - 80 °C

5: sodium carbonate; bis-triphenylphosphine-palladium(II) chloride / ethanol; toluene / 8 h / 100 °C

6: hydrogenchloride / methanol / 4 h / 100 °C

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; bromine; sodium hydride; sodium carbonate; hydrazine hydrate; acetic acid; In tetrahydrofuran; methanol; ethanol; toluene; mineral oil;