C₅₃H₇₀N₄O₄SSi₃

Base Information

Chemical Name:C₅₃H₇₀N₄O₄SSi₃
CAS No.:1434154-66-1
Molecular Formula:C₅₃H₇₀N₄O₄SSi₃
Molecular Weight:943.486
Hs Code.:

C<sub>53</sub>H<sub>70</sub>N<sub>4</sub>O<sub>4</sub>SSi<sub>3</sub>

Synonyms:C₅₃H₇₀N₄O₄SSi₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₃H₇₀N₄O₄SSi₃

Chemical Property:

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Technology Process of C₅₃H₇₀N₄O₄SSi₃

There total 10 articles about C₅₃H₇₀N₄O₄SSi₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1434154-36-5
((2R,3S,5R)-3-((tert-butyldiphenylsilyl)oxy)-5-((S)-2,2,9,9,10,10-hexamethyl-3,3-diphenyl-4,8-dioxa-3,9-disilaundecan-5-yl)tetrahydrofuran-2-yl)methanol

: 86-93-1
1-Phenyl-1H-tetrazole-5-thiol

: 1434154-66-1
C₅₃H₇₀N₄O₄SSi₃

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In toluene; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/jo4004647

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1434154-66-1
C₅₃H₇₀N₄O₄SSi₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: 1H-imidazole / dichloromethane / 6 h / 20 °C / Inert atmosphere

2.1: potassium carbonate / methanol / 20 h / 20 °C

3.1: titanium(IV) isopropylate; diethyl (2S,3S)-tartrate; tert.-butylhydroperoxide / dichloromethane; decane / 0.33 h / 20 °C / Inert atmosphere; Molecular sieve

3.2: -20 °C / Inert atmosphere

4.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran / 1 h / -30 - 0 °C / Inert atmosphere

5.1: 1H-imidazole / dichloromethane / 20 °C / Inert atmosphere

6.1: 1H-imidazole / 20 °C

7.1: ozone; oxygen / dichloromethane; methanol / -78 °C

7.2: 1 h / -78 - 20 °C

8.1: sodium tetrahydroborate / methanol / 1 h / 0 °C

9.1: triphenylphosphine; diethylazodicarboxylate / toluene / 3 h / 20 °C / Inert atmosphere

With 1H-imidazole; titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium tetrahydroborate; diethyl (2S,3S)-tartrate; oxygen; potassium carbonate; ozone; triphenylphosphine; sodium bis(2-methoxyethoxy)aluminium dihydride; diethylazodicarboxylate; In tetrahydrofuran; methanol; decane; dichloromethane; toluene; 3.1: |Sharpless Asymmetric Epoxidation / 9.1: |Mitsunobu Displacement;
DOI:10.1021/jo4004647

Reference yield:

: C₃₁H₄₈O₄Si₂

: 1434154-66-1
C₅₃H₇₀N₄O₄SSi₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1H-imidazole / 20 °C

2.1: ozone; oxygen / dichloromethane; methanol / -78 °C

2.2: 1 h / -78 - 20 °C

3.1: sodium tetrahydroborate / methanol / 1 h / 0 °C

4.1: triphenylphosphine; diethylazodicarboxylate / toluene / 3 h / 20 °C / Inert atmosphere

With 1H-imidazole; sodium tetrahydroborate; oxygen; ozone; triphenylphosphine; diethylazodicarboxylate; In methanol; dichloromethane; toluene; 4.1: |Mitsunobu Displacement;
DOI:10.1021/jo4004647