N-(2-acetylphenyl)-2-thiophenecarboxamide

Base Information

Chemical Name:N-(2-acetylphenyl)-2-thiophenecarboxamide
CAS No.:41242-35-7
Molecular Formula:C13H11NO2S
Molecular Weight:245.302
Hs Code.:
Mol file:41242-35-7.mol

Synonyms:N-(2-acetylphenyl)thiophene-2-carboxamide;N-(2-thenoyl)-2-acetylaniline;Thiophene-2-carboxylic acid (2-acetyl-phenyl)-amide;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-acetylphenyl)-2-thiophenecarboxamide

Chemical Property:

Vapor Pressure:0.000368mmHg at 25°C
Melting Point:127 - 130 °C
Boiling Point:318.2°C at 760 mmHg
Flash Point:146.2°C
PSA：74.41000
Density:1.295g/cm³
LogP:3.27600

Purity/Quality:

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Technology Process of N-(2-acetylphenyl)-2-thiophenecarboxamide

There total 4 articles about N-(2-acetylphenyl)-2-thiophenecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 5271-67-0
2-Thiophenecarbonyl chloride

: 551-93-9
2-aminoacetophenone

: 41242-35-7
N-(2-acetyl-phenyl)-2-thiophenecarboxamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/acs.orglett.6b02142

Reference yield: 82.0%

: 5813-89-8
2-thiophenylcarboxamide

: 2142-69-0
2-bromophenyl methyl ketone

: 41242-35-7
N-(2-acetyl-phenyl)-2-thiophenecarboxamide

Guidance literature:: With copper(l) iodide; potassium carbonate; N,N`-dimethylethylenediamine; 5A molecular sieve; In toluene; at 110 ℃; for 24h;
DOI:10.1021/jo701384n

Reference yield: 68.0%

: 527-72-0
2-thiophenylcarboxylic acid

: 551-93-9
2-aminoacetophenone

: 41242-35-7
N-(2-acetyl-phenyl)-2-thiophenecarboxamide

Guidance literature:: With triethylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1055/s-0030-1260198