2-methoxy-4-(4-methoxyphenyl)pyridine

Base Information

Chemical Name:2-methoxy-4-(4-methoxyphenyl)pyridine
CAS No.:1173157-41-9
Molecular Formula:C₁₃H₁₃NO₂
Molecular Weight:215.252
Hs Code.:

Synonyms:2-methoxy-4-(4-methoxyphenyl)pyridine

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Chemical Property of 2-methoxy-4-(4-methoxyphenyl)pyridine

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Technology Process of 2-methoxy-4-(4-methoxyphenyl)pyridine

There total 3 articles about 2-methoxy-4-(4-methoxyphenyl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 100367-39-3
4-bromo-2-methoxypyridine

: 696-62-8
para-iodoanisole

: 1173157-41-9
2-methoxy-4-(4-methoxyphenyl)pyridine

: 2132-80-1
4,4'-Dimethoxybiphenyl

Guidance literature:: With bis(tri-tert-butylphosphine)palladium⁽⁰⁾; (C₅H₅)2Zr(OC₄H₈)N(Si(CH₃)3)CH(C₆H₅); tri-tert-butyl phosphine; In toluene; at 80 ℃; for 16h; Sealed tube; Inert atmosphere;
DOI:10.1016/j.chempr.2021.06.007

Reference yield: 9.0%

: 2-methoxypyridine hydrochloride

: 104-94-9
4-methoxy-aniline

: 1173157-41-9
2-methoxy-4-(4-methoxyphenyl)pyridine

: 296776-83-5
2-methoxy-6-(4'-methoxyphenyl)pyridine

Guidance literature:: 4-methoxy-aniline; With tetrafluoroboric acid; sodium nitrite; In water; at 0 ℃; for 0.75h;

2-methoxypyridine hydrochloride; With oxygen; In water; at 20 ℃; for 48h; Sealed tube; Irradiation;
DOI:10.1021/acs.joc.9b01879

Reference yield:

: 100367-39-3
4-bromo-2-methoxypyridine

: 5720-07-0
4-methoxyphenylboronic acid

: 1173157-41-9
2-methoxy-4-(4-methoxyphenyl)pyridine

Guidance literature:: With potassium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In dimethyl sulfoxide; at 95 ℃; for 2h;