2-(S)-amino-3-(4-methoxyphenyl)-2-methylpropionamide

Base Information

Chemical Name:2-(S)-amino-3-(4-methoxyphenyl)-2-methylpropionamide
CAS No.:1299492-09-3
Molecular Formula:C₁₁H₁₆N₂O₂
Molecular Weight:208.26
Hs Code.:

Synonyms:2-(S)-amino-3-(4-methoxyphenyl)-2-methylpropionamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(S)-amino-3-(4-methoxyphenyl)-2-methylpropionamide

Chemical Property:

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Technology Process of 2-(S)-amino-3-(4-methoxyphenyl)-2-methylpropionamide

There total 3 articles about 2-(S)-amino-3-(4-methoxyphenyl)-2-methylpropionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1299492-08-2
2-[(R)-(carbamoylphenylmethyl)-amino]-3-(4-methoxyphenyl)-2-(S)-methylpropionamide

: 1299492-09-3
2-(S)-amino-3-(4-methoxyphenyl)-2-methylpropionamide

: 103-81-1
Benzeneacetamide

Guidance literature:: With ammonium formate; palladium on carbon; In isopropyl alcohol; for 1h; Product distribution / selectivity; Inert atmosphere; Reflux;

Reference yield:

: 122-84-9
4-methoxybenzyl methyl ketone

: 1299492-09-3
2-(S)-amino-3-(4-methoxyphenyl)-2-methylpropionamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: water; methanol / 20 h / 40 °C / Sealed tube

2.1: sulfuric acid / dichloromethane; water / 3.25 h / -10 - 0 °C / Cooling with ice

2.2: pH 8 - 9

3.1: ammonium formate / palladium on carbon / isopropyl alcohol / 1 h / Inert atmosphere; Reflux

With sulfuric acid; ammonium formate; palladium on carbon; In methanol; dichloromethane; water; isopropyl alcohol;

Reference yield:

: 1299492-07-1
2-[1-(S)-cyano-2-(4-methoxyphenyl)-1-methylethylamino]-2-(R)-phenylacetamide

: 1299492-09-3
2-(S)-amino-3-(4-methoxyphenyl)-2-methylpropionamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfuric acid / dichloromethane; water / 3.25 h / -10 - 0 °C / Cooling with ice

1.2: pH 8 - 9

2.1: ammonium formate / palladium on carbon / isopropyl alcohol / 1 h / Inert atmosphere; Reflux

With sulfuric acid; ammonium formate; palladium on carbon; In dichloromethane; water; isopropyl alcohol;