benzyl 6a-phenyl-3,3a,4,6-tetrahydro-1H-pyrrolo[3,4-c]isoxazole-5-carboxylate

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Chemical Name:benzyl 6a-phenyl-3,3a,4,6-tetrahydro-1H-pyrrolo[3,4-c]isoxazole-5-carboxylate
CAS No.:1463484-42-5
Molecular Formula:C₁₉H₂₀N₂O₃
Molecular Weight:324.379
Hs Code.:

Synonyms:benzyl 6a-phenyl-3,3a,4,6-tetrahydro-1H-pyrrolo[3,4-c]isoxazole-5-carboxylate

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Chemical Property of benzyl 6a-phenyl-3,3a,4,6-tetrahydro-1H-pyrrolo[3,4-c]isoxazole-5-carboxylate

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Technology Process of benzyl 6a-phenyl-3,3a,4,6-tetrahydro-1H-pyrrolo[3,4-c]isoxazole-5-carboxylate

There total 2 articles about benzyl 6a-phenyl-3,3a,4,6-tetrahydro-1H-pyrrolo[3,4-c]isoxazole-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1463484-39-0
benzyl 3,3a,4,6-tetrahydropyrrolo[3,4-c]isoxazole-5-carboxylate

: 100-58-3
phenylmagnesium bromide

: 1463484-42-5
benzyl 6a-phenyl-3,3a,4,6-tetrahydro-1H-pyrrolo[3,4-c]isoxazole-5-carboxylate

Guidance literature:: benzyl 3,3a,4,6-tetrahydropyrrolo[3,4-c]isoxazole-5-carboxylate; With boron trifluoride; In tetrahydrofuran; at -50 ℃; for 0.166667h;

phenylmagnesium bromide; In tetrahydrofuran; at -50 - 0 ℃; for 4h;

Reference yield:

: benzyl N-allyl-N-[(2E)-2-hydroxyiminoethyl]carbamate

: 1463484-42-5
benzyl 6a-phenyl-3,3a,4,6-tetrahydro-1H-pyrrolo[3,4-c]isoxazole-5-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hypochlorite / dichloromethane / 20 °C

2.1: boron trifluoride / tetrahydrofuran / 0.17 h / -50 °C

2.2: 4 h / -50 - 0 °C

With sodium hypochlorite; boron trifluoride; In tetrahydrofuran; dichloromethane;