5-[4-(1,2-cis-hexen-1-yl)tetrahydro-2H-pyran-4-yl]resorcinol

Base Information

Chemical Name:5-[4-(1,2-cis-hexen-1-yl)tetrahydro-2H-pyran-4-yl]resorcinol
CAS No.:1605281-06-8
Molecular Formula:C₁₇H₂₄O₃
Molecular Weight:276.376
Hs Code.:

Synonyms:5-[4-(1,2-cis-hexen-1-yl)tetrahydro-2H-pyran-4-yl]resorcinol

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Chemical Property of 5-[4-(1,2-cis-hexen-1-yl)tetrahydro-2H-pyran-4-yl]resorcinol

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Technology Process of 5-[4-(1,2-cis-hexen-1-yl)tetrahydro-2H-pyran-4-yl]resorcinol

There total 9 articles about 5-[4-(1,2-cis-hexen-1-yl)tetrahydro-2H-pyran-4-yl]resorcinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1605281-05-7
3,5-[bis(tert-butyldimethylsilyl)oxy]-1-[4-(1,2-cis-hexen-1-yl)tetrahydro-2H-pyran-4-yl]benzene

: 1605281-06-8
5-[4-(1,2-cis-hexen-1-yl)tetrahydro-2H-pyran-4-yl]resorcinol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere;

Reference yield:

: 58459-40-8
2-(3,5-dihydroxyphenyl)acetonitrile

: 1605281-06-8
5-[4-(1,2-cis-hexen-1-yl)tetrahydro-2H-pyran-4-yl]resorcinol

Guidance literature:: Multi-step reaction with 7 steps

1.1: toluene-4-sulfonic acid / diethyl ether / 1 h / 0 °C / Inert atmosphere

2.1: potassium hexamethylsilazane / tetrahydrofuran / 0.08 h / -16 °C / Inert atmosphere

2.2: 1 h / -16 °C / Inert atmosphere

3.1: toluene-4-sulfonic acid; methanol / 0.5 h / 25 °C

4.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 25 °C

5.1: diisobutylaluminium hydride / dichloromethane; toluene / 2.5 h / -78 °C / Inert atmosphere

6.1: tetrahydrofuran / 0.17 h / 10 °C

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

With 1H-imidazole; methanol; tetrabutyl ammonium fluoride; potassium hexamethylsilazane; diisobutylaluminium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 4-[3,5-bis(1-ethoxyethoxy)phenyl]tetrahydro-2H-pyran-4-carbonitrile

: 1605281-06-8
5-[4-(1,2-cis-hexen-1-yl)tetrahydro-2H-pyran-4-yl]resorcinol

Guidance literature:: Multi-step reaction with 5 steps

1: toluene-4-sulfonic acid; methanol / 0.5 h / 25 °C

2: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 25 °C

3: diisobutylaluminium hydride / dichloromethane; toluene / 2.5 h / -78 °C / Inert atmosphere

4: tetrahydrofuran / 0.17 h / 10 °C

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

With 1H-imidazole; methanol; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;