3,5-[bis(tert-butyldimethylsilyl)oxy]-1-[4-(1,2-cis-hexen-1-yl)tetrahydro-2H-pyran-4-yl]benzene

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Chemical Name:3,5-[bis(tert-butyldimethylsilyl)oxy]-1-[4-(1,2-cis-hexen-1-yl)tetrahydro-2H-pyran-4-yl]benzene
CAS No.:1605281-05-7
Molecular Formula:C₂₉H₅₂O₃Si₂
Molecular Weight:504.901
Hs Code.:

Synonyms:3,5-[bis(tert-butyldimethylsilyl)oxy]-1-[4-(1,2-cis-hexen-1-yl)tetrahydro-2H-pyran-4-yl]benzene

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Chemical Property of 3,5-[bis(tert-butyldimethylsilyl)oxy]-1-[4-(1,2-cis-hexen-1-yl)tetrahydro-2H-pyran-4-yl]benzene

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Technology Process of 3,5-[bis(tert-butyldimethylsilyl)oxy]-1-[4-(1,2-cis-hexen-1-yl)tetrahydro-2H-pyran-4-yl]benzene

There total 8 articles about 3,5-[bis(tert-butyldimethylsilyl)oxy]-1-[4-(1,2-cis-hexen-1-yl)tetrahydro-2H-pyran-4-yl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 29541-98-8,55317-64-1
pentylidenetriphenylphosphorane

: 1605281-04-6
4-[3,5-bis(tert-butyldimethylsilyloxy)phenyl]tetrahydro-2H-pyran-4-carboxaldehyde

: 1605281-05-7
3,5-[bis(tert-butyldimethylsilyl)oxy]-1-[4-(1,2-cis-hexen-1-yl)tetrahydro-2H-pyran-4-yl]benzene

Guidance literature:: In tetrahydrofuran; at 10 ℃; for 0.166667h;

Reference yield:

: 58459-40-8
2-(3,5-dihydroxyphenyl)acetonitrile

: 1605281-05-7
3,5-[bis(tert-butyldimethylsilyl)oxy]-1-[4-(1,2-cis-hexen-1-yl)tetrahydro-2H-pyran-4-yl]benzene

Guidance literature:: Multi-step reaction with 6 steps

1.1: toluene-4-sulfonic acid / diethyl ether / 1 h / 0 °C / Inert atmosphere

2.1: potassium hexamethylsilazane / tetrahydrofuran / 0.08 h / -16 °C / Inert atmosphere

2.2: 1 h / -16 °C / Inert atmosphere

3.1: toluene-4-sulfonic acid; methanol / 0.5 h / 25 °C

4.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 25 °C

5.1: diisobutylaluminium hydride / dichloromethane; toluene / 2.5 h / -78 °C / Inert atmosphere

6.1: tetrahydrofuran / 0.17 h / 10 °C

With 1H-imidazole; methanol; potassium hexamethylsilazane; diisobutylaluminium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1605281-02-4
4-(3,5-dihydroxyphenyl)tetrahydro-2H-pyran-4-carbonitrile

: 1605281-05-7
3,5-[bis(tert-butyldimethylsilyl)oxy]-1-[4-(1,2-cis-hexen-1-yl)tetrahydro-2H-pyran-4-yl]benzene

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 25 °C

2: diisobutylaluminium hydride / dichloromethane; toluene / 2.5 h / -78 °C / Inert atmosphere

3: tetrahydrofuran / 0.17 h / 10 °C

With 1H-imidazole; diisobutylaluminium hydride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;