2'',2'''-di-O-benzoyl-4'',6''-O-cyclohexylidene-3,2',6',3'',4'''-pentakis(N-tert-butoxucarbonyl)arbekacin

Base Information

Chemical Name:2'',2'''-di-O-benzoyl-4'',6''-O-cyclohexylidene-3,2',6',3'',4'''-pentakis(N-tert-butoxucarbonyl)arbekacin
CAS No.:189157-33-3
Molecular Formula:C₆₇H₁₀₀N₆O₂₂
Molecular Weight:1341.56
Hs Code.:

Synonyms:2'',2'''-di-O-benzoyl-4'',6''-O-cyclohexylidene-3,2',6',3'',4'''-pentakis(N-tert-butoxucarbonyl)arbekacin

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Chemical Property of 2'',2'''-di-O-benzoyl-4'',6''-O-cyclohexylidene-3,2',6',3'',4'''-pentakis(N-tert-butoxucarbonyl)arbekacin

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Technology Process of 2'',2'''-di-O-benzoyl-4'',6''-O-cyclohexylidene-3,2',6',3'',4'''-pentakis(N-tert-butoxucarbonyl)arbekacin

There total 3 articles about 2'',2'''-di-O-benzoyl-4'',6''-O-cyclohexylidene-3,2',6',3'',4'''-pentakis(N-tert-butoxucarbonyl)arbekacin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 98-88-4
benzoyl chloride

: 189157-32-2
4'',6''-O-cyclohexylidene-3,2',6',3'',4'''-pentakis(N-tert-butoxucarbonyl)arbekacin

: 189157-33-3
2'',2'''-di-O-benzoyl-4'',6''-O-cyclohexylidene-3,2',6',3'',4'''-pentakis(N-tert-butoxucarbonyl)arbekacin

Guidance literature:: With pyridine; for 2h; Ambient temperature;
DOI:10.1016/S0008-6215(96)00318-7

Reference yield:

: 933-40-4
cycloxexanone dimethyl ketal

: 189157-33-3
2'',2'''-di-O-benzoyl-4'',6''-O-cyclohexylidene-3,2',6',3'',4'''-pentakis(N-tert-butoxucarbonyl)arbekacin

Guidance literature:: Multi-step reaction with 2 steps

1: p-TsOH / dimethylformamide / 2 h / 50 °C / 30 Torr

2: 97 percent / pyridine / 2 h / Ambient temperature

With pyridine; toluene-4-sulfonic acid; In N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(96)00318-7

Reference yield:

: 189157-31-1
3,2',6',3'',4'''-pentakis(N-tert-butoxucarbonyl)arbekacin

: 189157-33-3
2'',2'''-di-O-benzoyl-4'',6''-O-cyclohexylidene-3,2',6',3'',4'''-pentakis(N-tert-butoxucarbonyl)arbekacin

Guidance literature:: Multi-step reaction with 2 steps

1: p-TsOH / dimethylformamide / 2 h / 50 °C / 30 Torr

2: 97 percent / pyridine / 2 h / Ambient temperature

With pyridine; toluene-4-sulfonic acid; In N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(96)00318-7