benzyl(2-isopropenyl)carbamyl chloride

Base Information

• Chemical Name: benzyl(2-isopropenyl)carbamyl chloride
• CAS No.: 324738-55-8
• Molecular Formula: C₁₇H₁₆ClNO
• Molecular Weight: 285.773
• Mol file: 324738-55-8.mol

Synonyms:benzyl(2-isopropenyl)carbamyl chloride

Chemical Property of benzyl(2-isopropenyl)carbamyl chloride

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of benzyl(2-isopropenyl)carbamyl chloride

There total 13 articles about benzyl(2-isopropenyl)carbamyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

phosgene (75-44-5) + N-benzyl-2-(prop-1-en-2-yl)benzen-amine (490035-95-5) → benzyl(2-isopropenyl)carbamyl chloride (324738-55-8)

Guidance literature:

With sodium hydrogencarbonate; In dichloromethane; water; toluene; at 0 - 20 ℃; for 0.166667h;

DOI:10.1016/j.jorganchem.2005.11.045

Reference yield:

bis(trichloromethyl) carbonate (32315-10-9) + N-benzyl-2-(prop-1-en-2-yl)benzen-amine (490035-95-5) → benzyl(2-isopropenyl)carbamyl chloride (324738-55-8)

Guidance literature:

With pyridine; In benzene; at 20 ℃;

DOI:10.1021/jo0602064

Reference yield:

2-isopropenylaniline (52562-19-3) → benzyl(2-isopropenyl)carbamyl chloride (324738-55-8)

Guidance literature:

Multi-step reaction with 3 steps

1: NaBH₄ / methanol

2: 76 percent / NaHCO₃ / CH₂Cl₂; H₂O; toluene / 0.17 h / 0 - 20 °C

With sodium tetrahydroborate; sodium hydrogencarbonate; In methanol; dichloromethane; water; toluene;

DOI:10.1016/j.jorganchem.2005.11.045

upstream raw materials:

phosgene

N-benzyl-2-(prop-1-en-2-yl)benzen-amine

bis(trichloromethyl) carbonate

2-isopropenylaniline

Downstream raw materials:

S-(4-pentynyl) N-benzyl-N-(2-isopropenylphenyl)carbamothioate

N-benzyl-N-[2-(prop-1-en-2-yl)phenyl]-1-cyanoformamide

(1-benzyl-3-methyl-2-oxo-2,3-dihydro-1H-indol-3-yl)acetonitrile

1-benzyl-4-methylquinolin-2(1H)-one