4,9-bis(p-tolylsulphonyl)benz-15,20-dioxa-1,4,9,12-tetra-azabicyclo<10.5.5>docosane

Base Information

Chemical Name:4,9-bis(p-tolylsulphonyl)benz-15,20-dioxa-1,4,9,12-tetra-azabicyclo<10.5.5>docosane
CAS No.:121031-84-3
Molecular Formula:C₃₄H₄₆N₄O₆S₂
Molecular Weight:670.894
Hs Code.:

4,9-bis(p-tolylsulphonyl)benz<f>-15,20-dioxa-1,4,9,12-tetra-azabicyclo<10.5.5>docosane

Synonyms:4,9-bis(p-tolylsulphonyl)benz-15,20-dioxa-1,4,9,12-tetra-azabicyclo<10.5.5>docosane

Suppliers and Price of 4,9-bis(p-tolylsulphonyl)benz-15,20-dioxa-1,4,9,12-tetra-azabicyclo<10.5.5>docosane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4,9-bis(p-tolylsulphonyl)benz-15,20-dioxa-1,4,9,12-tetra-azabicyclo<10.5.5>docosane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4,9-bis(p-tolylsulphonyl)benz-15,20-dioxa-1,4,9,12-tetra-azabicyclo<10.5.5>docosane

There total 3 articles about 4,9-bis(p-tolylsulphonyl)benz-15,20-dioxa-1,4,9,12-tetra-azabicyclo<10.5.5>docosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 118074-98-9
4,10-bis<2-(p-tolylsulphonylamino)ethyl>-1,7-dioxa-4,10-diazacyclododecane

: 91-13-4
α,α'-dibromo-o-xylene

: 121031-84-3
4,9-bis(p-tolylsulphonyl)benz-15,20-dioxa-1,4,9,12-tetra-azabicyclo<10.5.5>docosane

Guidance literature:: With sodium hydroxide; tetra-(n-butyl)ammonium iodide; Heating;

Reference yield:

: 294-92-8
diaza[12]crown-4

: 121031-84-3
4,9-bis(p-tolylsulphonyl)benz-15,20-dioxa-1,4,9,12-tetra-azabicyclo<10.5.5>docosane

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / acetonitrile / Heating

2: 71 percent / 45percent aq. NaOH, tetrabutylammonium iodide / Heating

With sodium hydroxide; tetra-(n-butyl)ammonium iodide; In acetonitrile;

Reference yield:

: 52601-77-1
4,10-bis(p-tolylsulphonyl)-1,7-dioxa-4,10-diazacyclododecane

: 121031-84-3
4,9-bis(p-tolylsulphonyl)benz-15,20-dioxa-1,4,9,12-tetra-azabicyclo<10.5.5>docosane

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / LiAlH₄ / tetrahydrofuran / 20 h / Heating

2: 92 percent / acetonitrile / 1 h / Heating

3: 71 percent / Bu₄NI, 50 percent aq. NaOH / toluene / 16 h / Heating

With sodium hydroxide; lithium aluminium tetrahydride; tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; toluene; acetonitrile;