N'-{[2,3-dichloro-6-(1,3-dioxolan-2-yl)phenyl]sulfonyl}acetohydrazide

Base Information

Chemical Name:N'-{[2,3-dichloro-6-(1,3-dioxolan-2-yl)phenyl]sulfonyl}acetohydrazide
CAS No.:1007116-50-8
Molecular Formula:C₁₁H₁₂Cl₂N₂O₅S
Molecular Weight:355.199
Hs Code.:

Synonyms:N'-{[2,3-dichloro-6-(1,3-dioxolan-2-yl)phenyl]sulfonyl}acetohydrazide

Suppliers and Price of N'-{[2,3-dichloro-6-(1,3-dioxolan-2-yl)phenyl]sulfonyl}acetohydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N'-{[2,3-dichloro-6-(1,3-dioxolan-2-yl)phenyl]sulfonyl}acetohydrazide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N'-{[2,3-dichloro-6-(1,3-dioxolan-2-yl)phenyl]sulfonyl}acetohydrazide

There total 4 articles about N'-{[2,3-dichloro-6-(1,3-dioxolan-2-yl)phenyl]sulfonyl}acetohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 6-(1,3-dioxolan-2-yl)-2,3-dichlorobenzenesulfonyl chloride

: 1068-57-1
acetic acid hydrazide

: 1007116-50-8
N'-{[2,3-dichloro-6-(1,3-dioxolan-2-yl)phenyl]sulfonyl}acetohydrazide

Guidance literature:: In isopropyl alcohol; at 0 - 20 ℃;
DOI:10.1016/j.tet.2013.11.058

Reference yield:

: C₉H₇Cl₂O₄S^(1-)*Li⁽¹⁺⁾

: 1007116-50-8
N'-{[2,3-dichloro-6-(1,3-dioxolan-2-yl)phenyl]sulfonyl}acetohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuryl dichloride / hexane / 2.17 h / -5 - 0 °C

2: isopropyl alcohol / 0 - 20 °C

With sulfuryl dichloride; In hexane; isopropyl alcohol;
DOI:10.1016/j.tet.2013.11.058

Reference yield:

: 6287-38-3
3,4-dichlorobenzaldehyde

: 1007116-50-8
N'-{[2,3-dichloro-6-(1,3-dioxolan-2-yl)phenyl]sulfonyl}acetohydrazide

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene-4-sulfonic acid / toluene / 6 h / Reflux; Dean-Stark

2.1: n-butyllithium / hexane; tetrahydrofuran / -78 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

3.1: sulfuryl dichloride / hexane / 2.17 h / -5 - 0 °C

4.1: isopropyl alcohol / 0 - 20 °C

With n-butyllithium; sulfuryl dichloride; toluene-4-sulfonic acid; In tetrahydrofuran; hexane; isopropyl alcohol; toluene;
DOI:10.1016/j.tet.2013.11.058