1-Amino-8-nitropyrene

Base Information

Chemical Name:1-Amino-8-nitropyrene
CAS No.:30269-02-4
Molecular Formula:C16H10 N2 O2
Molecular Weight:262.268
Hs Code.:2921499090
DSSTox Substance ID:DTXSID80184357
Nikkaji Number:J371.941C
Wikidata:Q83055291
ChEMBL ID:CHEMBL165270
Mol file:30269-02-4.mol

Synonyms:1-amino-8-nitropyrene;8-nitro-1-aminopyrene

Suppliers and Price of 1-Amino-8-nitropyrene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-AMINO-8-NITROPYRENE 95.00%
5MG
$ 499.48

Total 3 raw suppliers

Chemical Property of 1-Amino-8-nitropyrene

Chemical Property:

Vapor Pressure:1.32E-10mmHg at 25°C
Boiling Point:512.2°Cat760mmHg
Flash Point:263.6°C
PSA：71.84000
Density:1.489g/cm³
LogP:5.17880
XLogP3:4.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:262.074227566
Heavy Atom Count:20
Complexity:408

Purity/Quality:

99% ^*data from raw suppliers

1-AMINO-8-NITROPYRENE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC2=C3C(=C(C=C2)[N+](=O)[O-])C=CC4=C(C=CC1=C43)N

Technology Process of 1-Amino-8-nitropyrene

There total 1 articles about 1-Amino-8-nitropyrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1013-88-3
Benzophenone imine

: 1714-29-0
1-bromopyrene

: 30269-02-4
1-amino-8-nitropyrene

: 30269-01-3
1-amino-6-nitropyrene

: 1-amino-3-nitropyrene

Guidance literature:: 1-bromopyrene; With nitric acid; acetic acid; at 20 ℃; for 24h;

Benzophenone imine; With caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate; In tetrahydrofuran; for 16h; Heating;

With hydrogenchloride; In tetrahydrofuran; at 20 ℃; for 0.0833333h; Further stages.;
DOI:10.1021/ol000090c

Reference yield: 76.0%

: 30269-02-4
1-amino-8-nitropyrene

: 236427-58-0
2-bromo-6-benzyloxy-9-[2-deoxy-3,5-bis(O-tert-butyldimethylsilyl)-β-D-erythro-pentofuranosyl]purine

: 590409-48-6
2-(8-nitro-1-pyrenyl)-O⁶-benzyl-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyguanosine

Guidance literature:: With palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In toluene; at 80 ℃; for 16h;
DOI:10.1021/ol034904b

Reference yield:

: 30269-02-4
1-amino-8-nitropyrene

: 38303-35-4
1,8-dibromopyrene

Guidance literature:: Multi-step reaction with 3 steps

1: (i) NaNO₂, aq. H₂SO₄, DMF, (ii) CuBr, KBr, aq. HBr

2: N₂H₄*H₂O / Raney-Ni

3: (i) NaNO₂, aq. H₂SO₄, DMF, (ii) CuBr, KBr, aq. HBr

With hydrazine hydrate; nickel;