ethyl N-(cyanoacetyl)-N-[4-(2-methoxy-1,1-dimethyl-2-oxoethyl)phenyl]-beta-alaninate

Base Information

Chemical Name:ethyl N-(cyanoacetyl)-N-[4-(2-methoxy-1,1-dimethyl-2-oxoethyl)phenyl]-beta-alaninate
CAS No.:1236409-56-5
Molecular Formula:C₁₉H₂₄N₂O₅
Molecular Weight:360.41
Hs Code.:

Synonyms:ethyl N-(cyanoacetyl)-N-[4-(2-methoxy-1,1-dimethyl-2-oxoethyl)phenyl]-beta-alaninate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl N-(cyanoacetyl)-N-[4-(2-methoxy-1,1-dimethyl-2-oxoethyl)phenyl]-beta-alaninate

Chemical Property:

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Technology Process of ethyl N-(cyanoacetyl)-N-[4-(2-methoxy-1,1-dimethyl-2-oxoethyl)phenyl]-beta-alaninate

There total 1 articles about ethyl N-(cyanoacetyl)-N-[4-(2-methoxy-1,1-dimethyl-2-oxoethyl)phenyl]-beta-alaninate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1236409-53-2
ethyl N-[4-(2-methoxy-1,1-dimethyl-2-oxoethyl)phenyl]-beta-alaninate

: 372-09-8
cyanoacetic acid

: 1236409-56-5
ethyl N-(cyanoacetyl)-N-[4-(2-methoxy-1,1-dimethyl-2-oxoethyl)phenyl]-beta-alaninate

Guidance literature:: With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; triethylamine; In ethyl acetate; at 0 - 20 ℃; Product distribution / selectivity;

Reference yield:

: 1236409-56-5
ethyl N-(cyanoacetyl)-N-[4-(2-methoxy-1,1-dimethyl-2-oxoethyl)phenyl]-beta-alaninate

: 1236409-58-7
methyl 2-(4-(3-cyano-4-hydroxy-2-oxo-5,6-dihydropyridin-1(2H)-yl)phenyl)-2-methylpropanoate

Guidance literature:: ethyl N-(cyanoacetyl)-N-[4-(2-methoxy-1,1-dimethyl-2-oxoethyl)phenyl]-beta-alaninate; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol; at 70 ℃; for 2h;

With hydrogenchloride; water; In ethyl acetate; Product distribution / selectivity;