methyl 2-(4-(3-cyano-4-hydroxy-2-oxo-5,6-dihydropyridin-1(2H)-yl)phenyl)-2-methylpropanoate

Base Information

Chemical Name:methyl 2-(4-(3-cyano-4-hydroxy-2-oxo-5,6-dihydropyridin-1(2H)-yl)phenyl)-2-methylpropanoate
CAS No.:1236409-58-7
Molecular Formula:C₁₇H₁₈N₂O₄
Molecular Weight:314.341
Hs Code.:

Synonyms:methyl 2-(4-(3-cyano-4-hydroxy-2-oxo-5,6-dihydropyridin-1(2H)-yl)phenyl)-2-methylpropanoate

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Chemical Property of methyl 2-(4-(3-cyano-4-hydroxy-2-oxo-5,6-dihydropyridin-1(2H)-yl)phenyl)-2-methylpropanoate

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Technology Process of methyl 2-(4-(3-cyano-4-hydroxy-2-oxo-5,6-dihydropyridin-1(2H)-yl)phenyl)-2-methylpropanoate

There total 1 articles about methyl 2-(4-(3-cyano-4-hydroxy-2-oxo-5,6-dihydropyridin-1(2H)-yl)phenyl)-2-methylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1236409-56-5
ethyl N-(cyanoacetyl)-N-[4-(2-methoxy-1,1-dimethyl-2-oxoethyl)phenyl]-beta-alaninate

: 1236409-58-7
methyl 2-(4-(3-cyano-4-hydroxy-2-oxo-5,6-dihydropyridin-1(2H)-yl)phenyl)-2-methylpropanoate

Guidance literature:: ethyl N-(cyanoacetyl)-N-[4-(2-methoxy-1,1-dimethyl-2-oxoethyl)phenyl]-beta-alaninate; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol; at 70 ℃; for 2h;

With hydrogenchloride; water; In ethyl acetate; Product distribution / selectivity;

Reference yield: 87.0%

: 67-56-1
methanol

: 1236409-58-7
methyl 2-(4-(3-cyano-4-hydroxy-2-oxo-5,6-dihydropyridin-1(2H)-yl)phenyl)-2-methylpropanoate

: 1236409-59-8
methyl 2-(4-(3-cyano-4-methoxy-2-oxo-5,6-dihydropyridin-1(2H)-yl)phenyl)-2-methylpropanoate

Guidance literature:: methyl 2-(4-(3-cyano-4-hydroxy-2-oxo-5,6-dihydropyridin-1(2H)-yl)phenyl)-2-methylpropanoate; With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 0 - 20 ℃; for 1.33333h;

methanol; In dichloromethane; at 20 ℃; Product distribution / selectivity; Reflux;