palladium(II)(diphenylphosphinic acid(-2H))

Base Information

• Chemical Name: palladium(II)(diphenylphosphinic acid(-2H))
• CAS No.: 1332642-73-5
• Molecular Formula: C₁₂H₉O₂PPd
• Molecular Weight: 322.596
• Mol file: 1332642-73-5.mol

Synonyms:palladium(II)(diphenylphosphinic acid(-2H))

Chemical Property of palladium(II)(diphenylphosphinic acid(-2H))

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of palladium(II)(diphenylphosphinic acid(-2H))

There total 1 articles about palladium(II)(diphenylphosphinic acid(-2H)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

diphenyl-phosphinic acid (1707-03-5) + palladium diacetate (3375-31-3) → palladium(II)(diphenylphosphinic acid(-2H)) (1332642-73-5)

Guidance literature:

In tetrahydrofuran; heating mixt. of Pd salt and Ph2POOH in THF at 60°C; ppt. filtered, washed (THF), dried under vac.;

DOI:10.1039/c0cc03436c

Reference yield:

1,2-bis(dimethylphosphanyl)ethane (23936-60-9) + palladium(II)(diphenylphosphinic acid(-2H)) (1332642-73-5) → palladium(II)(diphenylphosphinic acid(-2H))(dmpe) (1278596-89-6)

Guidance literature:

In not given; mixing of Pd complex with dmpe;

DOI:10.1039/c0cc03436c

Reference yield:

1,2-bis(dimethylphosphanyl)ethane (23936-60-9) + palladium(II)(diphenylphosphinic acid(-2H)) (1332642-73-5) → [((C6H5)(C6H4)POOH)Pd((CH3)2PCH2CH2P(CH3)2)(P(C6H5)2O)]*CH2Cl2

Guidance literature:

Multi-step reaction with 2 steps

1: not given

2: dichloromethane

In dichloromethane;

DOI:10.1039/c0cc03436c

upstream raw materials:

diphenyl-phosphinic acid

palladium diacetate

Downstream raw materials:

palladium(II)(diphenylphosphinic acid(-2H))(dmpe)

palladium(II)(diphenylphosphinic acid(-2H))(dppe)