Technology Process of C14H9FN2
There total 3 articles about C14H9FN2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine; copper(l) iodide; trifluorormethanesulfonic acid; oxygen; copper(II) sulfate;
In
N,N-dimethyl-formamide;
at 110 ℃;
for 14h;
under 760.051 Torr;
DOI:10.1002/anie.201204339
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: acetic acid / ethanol / Reflux
2.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C
2.2: 5 h / 0 °C / Reflux
3.1: pyridine; copper(l) iodide; trifluorormethanesulfonic acid; oxygen; copper(II) sulfate / N,N-dimethyl-formamide / 14 h / 110 °C / 760.05 Torr
With
pyridine; copper(l) iodide; trifluorormethanesulfonic acid; oxygen; sodium hydride; copper(II) sulfate; acetic acid;
In
tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1002/anie.201204339
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: acetic acid / ethanol / Reflux
2.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C
2.2: 5 h / 0 °C / Reflux
3.1: pyridine; copper(l) iodide; trifluorormethanesulfonic acid; oxygen; copper(II) sulfate / N,N-dimethyl-formamide / 14 h / 110 °C / 760.05 Torr
With
pyridine; copper(l) iodide; trifluorormethanesulfonic acid; oxygen; sodium hydride; copper(II) sulfate; acetic acid;
In
tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1002/anie.201204339
