methyl 2-(3-(2-(tert-butylthiomethyl)-4-nitrophenoxy)-4-methoxyphenyl)acetate

Base Information

Chemical Name:methyl 2-(3-(2-(tert-butylthiomethyl)-4-nitrophenoxy)-4-methoxyphenyl)acetate
CAS No.:1313757-50-4
Molecular Formula:C₂₁H₂₅NO₆S
Molecular Weight:419.499
Hs Code.:

Synonyms:methyl 2-(3-(2-(tert-butylthiomethyl)-4-nitrophenoxy)-4-methoxyphenyl)acetate

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Chemical Property of methyl 2-(3-(2-(tert-butylthiomethyl)-4-nitrophenoxy)-4-methoxyphenyl)acetate

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Technology Process of methyl 2-(3-(2-(tert-butylthiomethyl)-4-nitrophenoxy)-4-methoxyphenyl)acetate

There total 5 articles about methyl 2-(3-(2-(tert-butylthiomethyl)-4-nitrophenoxy)-4-methoxyphenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1313757-49-1
methyl 2-(3-(2-bromomethyl-4-nitrophenoxy)-4-methoxyphenyl)acetate

: 75-66-1
2-methylpropan-2-thiol

: 1313757-50-4
methyl 2-(3-(2-(tert-butylthiomethyl)-4-nitrophenoxy)-4-methoxyphenyl)acetate

Guidance literature:: With sodium hydride; In tetrahydrofuran; mineral oil; at 0 - 15 ℃; for 5h;

Reference yield:

: 1131-94-8
homoisovanillic acid

: 1313757-50-4
methyl 2-(3-(2-(tert-butylthiomethyl)-4-nitrophenoxy)-4-methoxyphenyl)acetate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuric acid / 3.5 h / Reflux

2.1: potassium carbonate / 1,4-dioxane / 6 h / 70 °C

3.1: sodium tetrahydroborate / 1,4-dioxane; tetrahydrofuran / 10 - 20 °C

3.2: pH 2

4.1: phosphorus tribromide / 1,2-dimethoxyethane / 3 h / 25 - 50 °C

5.1: sodium hydride / tetrahydrofuran; mineral oil / 5 h / 0 - 15 °C

With sodium tetrahydroborate; phosphorus tribromide; sodium hydride; potassium carbonate; sulfuric acid; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; mineral oil;

Reference yield:

: 1313757-47-9
methyl 2-(3-(2-formyl-4-nitrophenoxy)-4-methoxyphenyl)acetate

: 1313757-50-4
methyl 2-(3-(2-(tert-butylthiomethyl)-4-nitrophenoxy)-4-methoxyphenyl)acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium tetrahydroborate / 1,4-dioxane; tetrahydrofuran / 10 - 20 °C

1.2: pH 2

2.1: phosphorus tribromide / 1,2-dimethoxyethane / 3 h / 25 - 50 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 5 h / 0 - 15 °C

With sodium tetrahydroborate; phosphorus tribromide; sodium hydride; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; mineral oil;