methyl 2-(3-(4-amino-2-(tert-butylthiomethyl)phenoxy)-4-methoxyphenyl)acetate

Base Information

Chemical Name:methyl 2-(3-(4-amino-2-(tert-butylthiomethyl)phenoxy)-4-methoxyphenyl)acetate
CAS No.:1313757-51-5
Molecular Formula:C₂₁H₂₇NO₄S
Molecular Weight:389.516
Hs Code.:

Synonyms:methyl 2-(3-(4-amino-2-(tert-butylthiomethyl)phenoxy)-4-methoxyphenyl)acetate

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Chemical Property of methyl 2-(3-(4-amino-2-(tert-butylthiomethyl)phenoxy)-4-methoxyphenyl)acetate

Chemical Property:

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Technology Process of methyl 2-(3-(4-amino-2-(tert-butylthiomethyl)phenoxy)-4-methoxyphenyl)acetate

There total 6 articles about methyl 2-(3-(4-amino-2-(tert-butylthiomethyl)phenoxy)-4-methoxyphenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1313757-50-4
methyl 2-(3-(2-(tert-butylthiomethyl)-4-nitrophenoxy)-4-methoxyphenyl)acetate

: 1313757-51-5
methyl 2-(3-(4-amino-2-(tert-butylthiomethyl)phenoxy)-4-methoxyphenyl)acetate

Guidance literature:: With N,N-Dimethylhydrazine; iron(III) chloride; In methanol; at 65 ℃; for 10h;

Reference yield:

: 15964-81-5
methyl 3-hydroxy-4-methoxyphenylacetate

: 1313757-51-5
methyl 2-(3-(4-amino-2-(tert-butylthiomethyl)phenoxy)-4-methoxyphenyl)acetate

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / 1,4-dioxane / 6 h / 70 °C

2.1: sodium tetrahydroborate / 1,4-dioxane; tetrahydrofuran / 10 - 20 °C

2.2: pH 2

3.1: phosphorus tribromide / 1,2-dimethoxyethane / 3 h / 25 - 50 °C

4.1: sodium hydride / tetrahydrofuran; mineral oil / 5 h / 0 - 15 °C

5.1: N,N-Dimethylhydrazine / iron(III) chloride / methanol / 10 h / 65 °C

With sodium tetrahydroborate; phosphorus tribromide; sodium hydride; potassium carbonate; N,N-Dimethylhydrazine; iron(III) chloride; In tetrahydrofuran; 1,4-dioxane; methanol; 1,2-dimethoxyethane; mineral oil;

Reference yield:

: 1131-94-8
homoisovanillic acid

: 1313757-51-5
methyl 2-(3-(4-amino-2-(tert-butylthiomethyl)phenoxy)-4-methoxyphenyl)acetate

Guidance literature:: Multi-step reaction with 6 steps

1.1: sulfuric acid / 3.5 h / Reflux

2.1: potassium carbonate / 1,4-dioxane / 6 h / 70 °C

3.1: sodium tetrahydroborate / 1,4-dioxane; tetrahydrofuran / 10 - 20 °C

3.2: pH 2

4.1: phosphorus tribromide / 1,2-dimethoxyethane / 3 h / 25 - 50 °C

5.1: sodium hydride / tetrahydrofuran; mineral oil / 5 h / 0 - 15 °C

6.1: N,N-Dimethylhydrazine / iron(III) chloride / methanol / 10 h / 65 °C

With sodium tetrahydroborate; phosphorus tribromide; sodium hydride; potassium carbonate; N,N-Dimethylhydrazine; iron(III) chloride; sulfuric acid; In tetrahydrofuran; 1,4-dioxane; methanol; 1,2-dimethoxyethane; mineral oil;