C₂₈H₁₈Cl₂N₆O₂S₂

Base Information

• Chemical Name: C₂₈H₁₈Cl₂N₆O₂S₂
• CAS No.: 1268364-61-9
• Molecular Formula: C₂₈H₁₈Cl₂N₆O₂S₂
• Molecular Weight: 605.528
• Mol file: 1268364-61-9.mol

Synonyms:C₂₈H₁₈Cl₂N₆O₂S₂

Chemical Property of C₂₈H₁₈Cl₂N₆O₂S₂

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₂₈H₁₈Cl₂N₆O₂S₂

There total 2 articles about C₂₈H₁₈Cl₂N₆O₂S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

2,2'-[1,3-phenylenebis(methan-1-yl-1-ylidene)]bis{N-[(dimethylamino)methylene]hydrazinecarbothioamide} + 4-chlorobenzoylmethyl bromide (536-38-9) → C28H18Cl2N6O2S2 (1268364-61-9)

Guidance literature:

2,2'-[1,3-phenylenebis(methan-1-yl-1-ylidene)]bis{N-[(dimethylamino)methylene]hydrazinecarbothioamide}; 4-chlorobenzoylmethyl bromide; In N,N-dimethyl-formamide; for 0.0333333h; Sealed tube;

With triethylamine; In N,N-dimethyl-formamide; at 20 - 50 ℃; for 0.166667h; Microwave irradiation; Sealed tube;

DOI:10.1002/cplu.201402031

Reference yield:

Isophthalaldehyde (626-19-7) → C28H18Cl2N6O2S2 (1268364-61-9)

Guidance literature:

Multi-step reaction with 3 steps

1: ethanol / 0.28 h / 20 - 120 °C / Microwave irradiation

2: ethanol; N,N-dimethyl-formamide / 0.15 h / 20 - 50 °C / Microwave irradiation

3: triethylamine / N,N-dimethyl-formamide / 0.15 h / 20 - 50 °C / Microwave irradiation

With triethylamine; In ethanol; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2010.12.072

Reference yield: 95.0%

C28H18Cl2N6O2S2 (1268364-61-9) + copper(II) acetate monohydrate (6046-93-1) → [5-(4-chlorobenzoyl)-2-{[3-({2-[5-(4-chlorobenzoyl)thiazol-2-yl]hydrazono}methyl)benzylidene]hydrazono}thiazol-3(2H)-yl]copper

Guidance literature:

In N,N-dimethyl-formamide; Microwave irradiation; Heating; Sealed tube;

DOI:10.1002/cplu.201402031

upstream raw materials:

4-chlorobenzoylmethyl bromide

Isophthalaldehyde