methyl 4-methoxy-2-(2,4,6-trimethoxyphenoxy)-6-methylbenzoate

Base Information

• Chemical Name: methyl 4-methoxy-2-(2,4,6-trimethoxyphenoxy)-6-methylbenzoate
• CAS No.: 81574-60-9
• Molecular Formula: C₁₉H₂₂O₇
• Molecular Weight: 362.379
• Mol file: 81574-60-9.mol

Synonyms:methyl 4-methoxy-2-(2,4,6-trimethoxyphenoxy)-6-methylbenzoate

Chemical Property of methyl 4-methoxy-2-(2,4,6-trimethoxyphenoxy)-6-methylbenzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of methyl 4-methoxy-2-(2,4,6-trimethoxyphenoxy)-6-methylbenzoate

There total 7 articles about methyl 4-methoxy-2-(2,4,6-trimethoxyphenoxy)-6-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

methyl 2-(4-hydroxy-2,6-dimethoxyphenoxy)-4-methoxy-6-methylbenzoate (81574-62-1) + methyl iodide (74-88-4) → methyl 4-methoxy-2-(2,4,6-trimethoxyphenoxy)-6-methylbenzoate (81574-60-9)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; Ambient temperature;

Reference yield: 59.0%

2,4,6-trimethoxyphenol (20491-92-3) + methyl 2-bromo-4-methoxy-6-methylbenzoate (55366-03-5) → methyl 4-methoxy-2-(2,4,6-trimethoxyphenoxy)-6-methylbenzoate (81574-60-9)

Guidance literature:

With potassium carbonate; copper(II) oxide; In pyridine; at 140 ℃; for 15h;

Reference yield:

2',6,6'-trimethoxy-4-methylspiro-3(2H),4'-dione (74628-35-6) → methyl 4-methoxy-2-(2,4,6-trimethoxyphenoxy)-6-methylbenzoate (81574-60-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 86 percent / methanol / 1 h / Heating

2: 91 percent / potassium carbonate / dimethylformamide / Ambient temperature

With potassium carbonate; In methanol; N,N-dimethyl-formamide;

upstream raw materials:

2,4,6-trimethoxyphenol

methyl 2-bromo-4-methoxy-6-methylbenzoate

methyl 2-(4-hydroxy-2,6-dimethoxyphenoxy)-4-methoxy-6-methylbenzoate

methyl iodide

Downstream raw materials:

2-hydroxy-2',4,4'6'-tetramethoxy-6-methylbenzophenone

2,4'-dihydroxy-2',4,6'-trimethoxy-6-methylbenzophenone

1,3,6-trimethoxy-8-methyl-9H-xanthen-9-one

lichenxanthone