C₁₉H₁₅NO₃

Base Information

Chemical Name:C₁₉H₁₅NO₃
CAS No.:127766-74-9
Molecular Formula:C₁₉H₁₅NO₃
Molecular Weight:305.333
Hs Code.:

C<sub>19</sub>H<sub>15</sub>NO<sub>3</sub>

Synonyms:C₁₉H₁₅NO₃

Suppliers and Price of C₁₉H₁₅NO₃

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Chemical Property of C₁₉H₁₅NO₃

Chemical Property:

Purity/Quality:

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Technology Process of C₁₉H₁₅NO₃

There total 19 articles about C₁₉H₁₅NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 127766-61-4,127995-48-6,133099-18-0
C₁₉H₁₇NO₄

: 127766-74-9
C₁₉H₁₅NO₃

Guidance literature:: With quinoline; camphor-10-sulfonic acid; In benzene; Heating;
DOI:10.1016/S0040-4039(01)89002-X

Reference yield:

: 5344-90-1
2-Aminobenzyl alcohol

: 127766-74-9
C₁₉H₁₅NO₃

Guidance literature:: Multi-step reaction with 19 steps

1: HNO₂, NaN₃

2: PCC

3: NaOH

4: 100 percent / n-Bu₄NF / tetrahydrofuran / -78 °C

5: 85 percent / BF₃-Et₂O / CH₂Cl₂

6: 81 percent / ethanol

7: 91 percent / Ph₃P, AcOH / methanol; tetrahydrofuran / 23 °C

8: 1.) DIBAL, 2.) NaBH₃CN, TFA / 1.) CH₂Cl₂, -78 deg C, 2.) MeOH, CH₂Cl₂

9: pyridine / CH₂Cl₂

10: pyridine

11: 99 percent / HgCl₂ / methanol / Heating

12: MCPBA / CH₂Cl₂

13: toluene / 175 °C

14: 70 percent / NaOH/H₂O / methanol / Heating

15: 89 percent / 2-(phenylsulfonyl)-3-phenyloxaziridine (Davis' reagent) / tetrahydrofuran / 23 °C

16: 85 percent / 23 °C

17: 78 percent / MCPBA, NaHCO₃ / CH₂Cl₂ / 23 °C

18: 1.) (COCl)2, Et₃N, 2.) H₂NNH₂ / 1.) DMSO, CH₂Cl₂, -78 deg C, 2.) MeOH, CH₂Cl₂, 0 deg C

19: 60 percent / CSA, quinoline / benzene / Heating

With pyridine; quinoline; sodium hydroxide; sodium azide; oxalyl dichloride; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; water; cis-nitrous acid; diisobutylaluminium hydride; sodium cyanoborohydride; sodium hydrogencarbonate; acetic acid; N-(benzenesulfonyl)-3-phenyloxaziridine; triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; pyridinium chlorochromate; trifluoroacetic acid; mercury dichloride; hydrazine; In tetrahydrofuran; methanol; ethanol; dichloromethane; toluene; benzene;
DOI:10.1016/S0040-4039(01)89002-X

Reference yield:

: 33037-74-0
(E)-3-(2-azidophenyl)-1-phenylprop-2-en-1-one

: 127766-74-9
C₁₉H₁₅NO₃

Guidance literature:: Multi-step reaction with 16 steps

1: 100 percent / n-Bu₄NF / tetrahydrofuran / -78 °C

2: 85 percent / BF₃-Et₂O / CH₂Cl₂

3: 81 percent / ethanol

4: 91 percent / Ph₃P, AcOH / methanol; tetrahydrofuran / 23 °C

5: 1.) DIBAL, 2.) NaBH₃CN, TFA / 1.) CH₂Cl₂, -78 deg C, 2.) MeOH, CH₂Cl₂

6: pyridine / CH₂Cl₂

7: pyridine

8: 99 percent / HgCl₂ / methanol / Heating

9: MCPBA / CH₂Cl₂

10: toluene / 175 °C

11: 70 percent / NaOH/H₂O / methanol / Heating

12: 89 percent / 2-(phenylsulfonyl)-3-phenyloxaziridine (Davis' reagent) / tetrahydrofuran / 23 °C

13: 85 percent / 23 °C

14: 78 percent / MCPBA, NaHCO₃ / CH₂Cl₂ / 23 °C

15: 1.) (COCl)2, Et₃N, 2.) H₂NNH₂ / 1.) DMSO, CH₂Cl₂, -78 deg C, 2.) MeOH, CH₂Cl₂, 0 deg C

16: 60 percent / CSA, quinoline / benzene / Heating

With pyridine; quinoline; sodium hydroxide; oxalyl dichloride; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; water; diisobutylaluminium hydride; sodium cyanoborohydride; sodium hydrogencarbonate; acetic acid; N-(benzenesulfonyl)-3-phenyloxaziridine; triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; trifluoroacetic acid; mercury dichloride; hydrazine; In tetrahydrofuran; methanol; ethanol; dichloromethane; toluene; benzene;
DOI:10.1016/S0040-4039(01)89002-X