C₂₀H₁₈ClFN₄O₄S

Base Information

Chemical Name:C₂₀H₁₈ClFN₄O₄S
CAS No.:1421918-01-5
Molecular Formula:C₂₀H₁₈ClFN₄O₄S
Molecular Weight:464.905
Hs Code.:

C<sub>20</sub>H<sub>18</sub>ClFN<sub>4</sub>O<sub>4</sub>S

Synonyms:C₂₀H₁₈ClFN₄O₄S

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Chemical Property of C₂₀H₁₈ClFN₄O₄S

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Technology Process of C₂₀H₁₈ClFN₄O₄S

There total 7 articles about C₂₀H₁₈ClFN₄O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 945396-72-5
2-chloro-N-(5-chlorobenzo[d][1,3]dioxol-4-yl)pyrimidin-4-amine

: 1421918-00-4
3-(3-fluoropropylsulfonyl)aniline

: 1421918-01-5
C₂₀H₁₈ClFN₄O₄S

Guidance literature:: With toluene-4-sulfonic acid; In 1,4-dioxane; at 100 ℃; for 48h;
DOI:10.1002/cmdc.201200264

Reference yield:

: 379228-45-2
5-chlorobenzo[d][1,3]dioxolcyclopenten-4-amine

: 1421918-01-5
C₂₀H₁₈ClFN₄O₄S

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / mineral oil; tetrahydrofuran / 1 h / 0 °C / Schlenk technique; Inert atmosphere

2: toluene-4-sulfonic acid / 1,4-dioxane / 48 h / 100 °C

With sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; 1,4-dioxane; mineral oil;
DOI:10.1002/cmdc.201200264

Reference yield:

: 25062-90-2
3-phenylsulfonylpropanol

: 1421918-01-5
C₂₀H₁₈ClFN₄O₄S

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine; dmap / dichloromethane / 20 °C

2: cesium fluoride; tert-butyl alcohol / 3 h / 70 °C

3: potassium nitrate; sulfuric acid / 6 h / 70 °C

4: palladium on activated charcoal; hydrogen / methanol / 16 h / 20 °C / 1125.11 - 1500.15 Torr

5: toluene-4-sulfonic acid / 1,4-dioxane / 48 h / 100 °C

With dmap; sulfuric acid; palladium on activated charcoal; hydrogen; toluene-4-sulfonic acid; potassium nitrate; triethylamine; cesium fluoride; tert-butyl alcohol; In 1,4-dioxane; methanol; dichloromethane;
DOI:10.1002/cmdc.201200264