1,1'-[2,5,8,11,14-pentaoxapentadecane-1,15-diylbis(2-methoxy-4,1-phenylene)]dipiperazine

Base Information

Chemical Name:1,1'-[2,5,8,11,14-pentaoxapentadecane-1,15-diylbis(2-methoxy-4,1-phenylene)]dipiperazine
CAS No.:1355460-62-6
Molecular Formula:C₃₂H₅₀N₄O₇
Molecular Weight:602.772
Hs Code.:

Synonyms:1,1'-[2,5,8,11,14-pentaoxapentadecane-1,15-diylbis(2-methoxy-4,1-phenylene)]dipiperazine

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Chemical Property of 1,1'-[2,5,8,11,14-pentaoxapentadecane-1,15-diylbis(2-methoxy-4,1-phenylene)]dipiperazine

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Technology Process of 1,1'-[2,5,8,11,14-pentaoxapentadecane-1,15-diylbis(2-methoxy-4,1-phenylene)]dipiperazine

There total 2 articles about 1,1'-[2,5,8,11,14-pentaoxapentadecane-1,15-diylbis(2-methoxy-4,1-phenylene)]dipiperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 37860-51-8
tetraethylene glycol di(p-toluenesulfonate)

: 1355460-62-6
1,1'-[2,5,8,11,14-pentaoxapentadecane-1,15-diylbis(2-methoxy-4,1-phenylene)]dipiperazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; paraffin oil / 0.25 h / 0 °C

1.2: 0 - 20 °C

2.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; johnphos; sodium t-butanolate / toluene / 18 h / 115 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium hydride; johnphos; sodium t-butanolate; In tetrahydrofuran; toluene; paraffin oil;
DOI:10.1016/j.bmc.2011.10.063

Reference yield:

: 17100-64-0
(4-bromo-3-methoxyphenyl)methanol

: 1355460-62-6
1,1'-[2,5,8,11,14-pentaoxapentadecane-1,15-diylbis(2-methoxy-4,1-phenylene)]dipiperazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; paraffin oil / 0.25 h / 0 °C

1.2: 0 - 20 °C

2.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; johnphos; sodium t-butanolate / toluene / 18 h / 115 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium hydride; johnphos; sodium t-butanolate; In tetrahydrofuran; toluene; paraffin oil;
DOI:10.1016/j.bmc.2011.10.063