(3R,4S,5R)-2-Methoxy-4-(4-methoxy-benzyloxy)-5-octyl-3-prop-2-ynyloxy-tetrahydro-furan

Base Information

Chemical Name:(3R,4S,5R)-2-Methoxy-4-(4-methoxy-benzyloxy)-5-octyl-3-prop-2-ynyloxy-tetrahydro-furan
CAS No.:130890-38-9
Molecular Formula:C₂₄H₃₆O₅
Molecular Weight:404.547
Hs Code.:

Synonyms:(3R,4S,5R)-2-Methoxy-4-(4-methoxy-benzyloxy)-5-octyl-3-prop-2-ynyloxy-tetrahydro-furan

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Chemical Property of (3R,4S,5R)-2-Methoxy-4-(4-methoxy-benzyloxy)-5-octyl-3-prop-2-ynyloxy-tetrahydro-furan

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Technology Process of (3R,4S,5R)-2-Methoxy-4-(4-methoxy-benzyloxy)-5-octyl-3-prop-2-ynyloxy-tetrahydro-furan

There total 3 articles about (3R,4S,5R)-2-Methoxy-4-(4-methoxy-benzyloxy)-5-octyl-3-prop-2-ynyloxy-tetrahydro-furan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 130890-37-8
(3R,4R,5R)-2-Methoxy-4-(4-methoxy-benzyloxy)-5-octyl-tetrahydro-furan-3-ol

: 106-96-7
propargyl bromide

: 130890-38-9
(3R,4S,5R)-2-Methoxy-4-(4-methoxy-benzyloxy)-5-octyl-3-prop-2-ynyloxy-tetrahydro-furan

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 2h; Ambient temperature;
DOI:10.1016/S0040-4039(00)97772-4

Reference yield:

: 130890-35-6
(3aR,5R,6S,6aR)-6-(4-Methoxy-benzyloxy)-2,2-dimethyl-5-((Z)-oct-1-enyl)-tetrahydro-furo[2,3-d][1,3]dioxole

: 130890-38-9
(3R,4S,5R)-2-Methoxy-4-(4-methoxy-benzyloxy)-5-octyl-3-prop-2-ynyloxy-tetrahydro-furan

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / 10percent Pd/C / ethanol / 6 h / 760 Torr / Ambient temperature

2: 80 percent / Amberlite IR 120 H+ / 12 h / 80 °C

3: 80 percent / NaH / tetrahydrofuran / 2 h / Ambient temperature

With Amberlite IR 120 H+; hydrogen; sodium hydride; palladium on activated charcoal; In tetrahydrofuran; ethanol;
DOI:10.1016/S0040-4039(00)97772-4

Reference yield:

: 130890-36-7
(3aR,5R,6S,6aR)-6-(4-Methoxy-benzyloxy)-2,2-dimethyl-5-octyl-tetrahydro-furo[2,3-d][1,3]dioxole

: 130890-38-9
(3R,4S,5R)-2-Methoxy-4-(4-methoxy-benzyloxy)-5-octyl-3-prop-2-ynyloxy-tetrahydro-furan

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / Amberlite IR 120 H+ / 12 h / 80 °C

2: 80 percent / NaH / tetrahydrofuran / 2 h / Ambient temperature

With Amberlite IR 120 H+; sodium hydride; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)97772-4