(3aR,5R,6S,6aR)-6-(4-Methoxy-benzyloxy)-2,2-dimethyl-5-((Z)-oct-1-enyl)-tetrahydro-furo[2,3-d][1,3]dioxole

Base Information

Chemical Name:(3aR,5R,6S,6aR)-6-(4-Methoxy-benzyloxy)-2,2-dimethyl-5-((Z)-oct-1-enyl)-tetrahydro-furo[2,3-d][1,3]dioxole
CAS No.:130890-35-6
Molecular Formula:C₂₃H₃₄O₅
Molecular Weight:390.52
Hs Code.:

Synonyms:(3aR,5R,6S,6aR)-6-(4-Methoxy-benzyloxy)-2,2-dimethyl-5-((Z)-oct-1-enyl)-tetrahydro-furo[2,3-d][1,3]dioxole

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Chemical Property of (3aR,5R,6S,6aR)-6-(4-Methoxy-benzyloxy)-2,2-dimethyl-5-((Z)-oct-1-enyl)-tetrahydro-furo[2,3-d][1,3]dioxole

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Technology Process of (3aR,5R,6S,6aR)-6-(4-Methoxy-benzyloxy)-2,2-dimethyl-5-((Z)-oct-1-enyl)-tetrahydro-furo[2,3-d][1,3]dioxole

There total 1 articles about (3aR,5R,6S,6aR)-6-(4-Methoxy-benzyloxy)-2,2-dimethyl-5-((Z)-oct-1-enyl)-tetrahydro-furo[2,3-d][1,3]dioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13423-48-8
triphenylheptylphosphonium bromide

: 82529-87-1
(3aR,5S,6S,6aR)-6-(4-methoxybenzyloxy)-tetrahydro-2,2-dimethylfuro[2,3-d][1,3]dioxole-5-carbaldehyde

: 130890-35-6
(3aR,5R,6S,6aR)-6-(4-Methoxy-benzyloxy)-2,2-dimethyl-5-((Z)-oct-1-enyl)-tetrahydro-furo[2,3-d][1,3]dioxole

Guidance literature:: With n-butyllithium; Multistep reaction; THF, r.t.;
DOI:10.1016/S0040-4039(00)97772-4

Reference yield:

: 130890-35-6
(3aR,5R,6S,6aR)-6-(4-Methoxy-benzyloxy)-2,2-dimethyl-5-((Z)-oct-1-enyl)-tetrahydro-furo[2,3-d][1,3]dioxole

: 130890-36-7
(3aR,5R,6S,6aR)-6-(4-Methoxy-benzyloxy)-2,2-dimethyl-5-octyl-tetrahydro-furo[2,3-d][1,3]dioxole

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 6h; under 760 Torr; Yield given; Ambient temperature;
DOI:10.1016/S0040-4039(00)97772-4

Reference yield:

: 130890-35-6
(3aR,5R,6S,6aR)-6-(4-Methoxy-benzyloxy)-2,2-dimethyl-5-((Z)-oct-1-enyl)-tetrahydro-furo[2,3-d][1,3]dioxole

: 130890-37-8
(3R,4R,5R)-2-Methoxy-4-(4-methoxy-benzyloxy)-5-octyl-tetrahydro-furan-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C / ethanol / 6 h / 760 Torr / Ambient temperature

2: 80 percent / Amberlite IR 120 H+ / 12 h / 80 °C

With Amberlite IR 120 H+; hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1016/S0040-4039(00)97772-4