1-[3,5-bis(6-aminopyridin-2-yl)carbamoyl]phenyl-2,6-dimethyl-4-pyridone

Base Information

Chemical Name:1-[3,5-bis(6-aminopyridin-2-yl)carbamoyl]phenyl-2,6-dimethyl-4-pyridone
CAS No.:905267-71-2
Molecular Formula:C₂₅H₂₃N₇O₃
Molecular Weight:469.503
Hs Code.:

Synonyms:1-[3,5-bis(6-aminopyridin-2-yl)carbamoyl]phenyl-2,6-dimethyl-4-pyridone

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Chemical Property of 1-[3,5-bis(6-aminopyridin-2-yl)carbamoyl]phenyl-2,6-dimethyl-4-pyridone

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Technology Process of 1-[3,5-bis(6-aminopyridin-2-yl)carbamoyl]phenyl-2,6-dimethyl-4-pyridone

There total 4 articles about 1-[3,5-bis(6-aminopyridin-2-yl)carbamoyl]phenyl-2,6-dimethyl-4-pyridone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 905267-70-1
1-(3,5-dicarbethoxy)phenyl-2,6-dimethyl-4-pyridone

: 141-86-6
2.6-diaminopyridine

: 905267-71-2
1-[3,5-bis(6-aminopyridin-2-yl)carbamoyl]phenyl-2,6-dimethyl-4-pyridone

Guidance literature:: With tert.-butyl lithium; In tetrahydrofuran; pentane; at -78 - 20 ℃;
DOI:10.1021/jo801083b

Reference yield:

: 1-(3,5-dicarboxy)phenyl-2,6-dimethyl-4-pyridone hydrochloride

: 905267-71-2
1-[3,5-bis(6-aminopyridin-2-yl)carbamoyl]phenyl-2,6-dimethyl-4-pyridone

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / H₂SO₄ / toluene / 6 h / Heating

2: 55 percent / t-BuLi / tetrahydrofuran / 20 h / 20 °C

With sulfuric acid; tert.-butyl lithium; In tetrahydrofuran; toluene;
DOI:10.1002/anie.200504581

Reference yield:

: 99-31-0
5-aminoisophthalic acid

: 905267-71-2
1-[3,5-bis(6-aminopyridin-2-yl)carbamoyl]phenyl-2,6-dimethyl-4-pyridone

Guidance literature:: Multi-step reaction with 3 steps

1: 53 percent / HCl / H₂O / 15 h / 110 °C

2: 82 percent / H₂SO₄ / toluene / 6 h / Heating

3: 55 percent / t-BuLi / tetrahydrofuran / 20 h / 20 °C

With hydrogenchloride; sulfuric acid; tert.-butyl lithium; In tetrahydrofuran; water; toluene;
DOI:10.1002/anie.200504581