N'-[2-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-propionyl]-hydrazinecarboxylic acid benzyl ester

Base Information

Chemical Name:N'-[2-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-propionyl]-hydrazinecarboxylic acid benzyl ester
CAS No.:77176-16-0
Molecular Formula:C₁₉H₁₇N₃O₅
Molecular Weight:367.361
Hs Code.:

Synonyms:N'-[2-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-propionyl]-hydrazinecarboxylic acid benzyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N'-[2-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-propionyl]-hydrazinecarboxylic acid benzyl ester

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Technology Process of N'-[2-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-propionyl]-hydrazinecarboxylic acid benzyl ester

There total 2 articles about N'-[2-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-propionyl]-hydrazinecarboxylic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 5331-43-1
N-benzyloxycarbonyl-hydrazine

: 53701-47-6
2-(1,3-dioxoisoindolin-2-yl)propanoyl chloride

: 77176-16-0
N'-[2-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-propionyl]-hydrazinecarboxylic acid benzyl ester

Guidance literature:: In ethyl acetate; at 0 - 25 ℃;
DOI:10.1002/hlca.19800630707

Reference yield:

: 21860-84-4
2-phthalimidopropionic acid

: 77176-16-0
N'-[2-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-propionyl]-hydrazinecarboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: PCl₅

2: 89 percent / ethyl acetate / 0 - 25 °C

With phosphorus pentachloride; In ethyl acetate;
DOI:10.1002/hlca.19800630707