DL-(1,2,4/3,5)-4-O-benzoyl-5-benzoyloxymethyl-1,2,3-tri-O-benzyl-1,2,3,4-cyclohexanetetrol

Base Information

Chemical Name:DL-(1,2,4/3,5)-4-O-benzoyl-5-benzoyloxymethyl-1,2,3-tri-O-benzyl-1,2,3,4-cyclohexanetetrol
CAS No.:125258-19-7
Molecular Formula:C₄₂H₄₀O₇
Molecular Weight:656.775
Hs Code.:

Synonyms:DL-(1,2,4/3,5)-4-O-benzoyl-5-benzoyloxymethyl-1,2,3-tri-O-benzyl-1,2,3,4-cyclohexanetetrol

Suppliers and Price of DL-(1,2,4/3,5)-4-O-benzoyl-5-benzoyloxymethyl-1,2,3-tri-O-benzyl-1,2,3,4-cyclohexanetetrol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of DL-(1,2,4/3,5)-4-O-benzoyl-5-benzoyloxymethyl-1,2,3-tri-O-benzyl-1,2,3,4-cyclohexanetetrol

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of DL-(1,2,4/3,5)-4-O-benzoyl-5-benzoyloxymethyl-1,2,3-tri-O-benzyl-1,2,3,4-cyclohexanetetrol

There total 6 articles about DL-(1,2,4/3,5)-4-O-benzoyl-5-benzoyloxymethyl-1,2,3-tri-O-benzyl-1,2,3,4-cyclohexanetetrol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 532-32-1
sodium benzoate

: 125258-16-4
DL-(1,2/3,4,5)-1,2,3-tri-O-benzyl-4-O-methanesulfonyl-5-methanesulfonyloxymethyl-1,2,3,4-cyclohexanetetrol

: 125258-19-7
DL-(1,2,4/3,5)-4-O-benzoyl-5-benzoyloxymethyl-1,2,3-tri-O-benzyl-1,2,3,4-cyclohexanetetrol

Guidance literature:: In N,N-dimethyl-formamide; at 120 ℃;
DOI:10.1016/0008-6215(89)85057-8

Reference yield: 88.0%

: 532-32-1
sodium benzoate

: 125258-15-3
Benzoic acid (1S,2R,3S,4R,5R)-3,4,5-tris-benzyloxy-2-methanesulfonyloxy-cyclohexylmethyl ester

: 125258-19-7
DL-(1,2,4/3,5)-4-O-benzoyl-5-benzoyloxymethyl-1,2,3-tri-O-benzyl-1,2,3,4-cyclohexanetetrol

Guidance literature:: In N,N-dimethyl-formamide; at 120 ℃; for 4h;
DOI:10.1016/0008-6215(89)85057-8

Reference yield:

: 117902-49-5
(1RS,6RS,8RS,9SR,10SR)-8,9,10-trobenzyloxy-3,3-dimethyl-2,4-dioxabicyclo<4.4.0>decane

: 125258-19-7
DL-(1,2,4/3,5)-4-O-benzoyl-5-benzoyloxymethyl-1,2,3-tri-O-benzyl-1,2,3,4-cyclohexanetetrol

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / 50percent AcOH, / ethanol; H₂O / 3.5 h / Ambient temperature

2: 83 percent / pyridine / 15 h / 40 °C

3: 83 percent / pyridine / 48 h / 45 °C

4: 88 percent / dimethylformamide / 4 h / 120 °C

With acetic acid; In pyridine; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(89)85057-8