Benzoic acid (1S,2R,3S,4R,5R)-3,4,5-tris-benzyloxy-2-methanesulfonyloxy-cyclohexylmethyl ester

Base Information

Chemical Name:Benzoic acid (1S,2R,3S,4R,5R)-3,4,5-tris-benzyloxy-2-methanesulfonyloxy-cyclohexylmethyl ester
CAS No.:125258-15-3
Molecular Formula:C₃₆H₃₈O₈S
Molecular Weight:630.759
Hs Code.:

Synonyms:Benzoic acid (1S,2R,3S,4R,5R)-3,4,5-tris-benzyloxy-2-methanesulfonyloxy-cyclohexylmethyl ester

Suppliers and Price of Benzoic acid (1S,2R,3S,4R,5R)-3,4,5-tris-benzyloxy-2-methanesulfonyloxy-cyclohexylmethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Benzoic acid (1S,2R,3S,4R,5R)-3,4,5-tris-benzyloxy-2-methanesulfonyloxy-cyclohexylmethyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of Benzoic acid (1S,2R,3S,4R,5R)-3,4,5-tris-benzyloxy-2-methanesulfonyloxy-cyclohexylmethyl ester

There total 4 articles about Benzoic acid (1S,2R,3S,4R,5R)-3,4,5-tris-benzyloxy-2-methanesulfonyloxy-cyclohexylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 124-63-0
methanesulfonyl chloride

: 125258-13-1,125354-36-1
DL-(1,2/3,4,5)-5-benzyloxymethyl-1,2,3-tri-O-benzyl-1,2,3,4-cyclohexanetetrol

: 125258-15-3
Benzoic acid (1S,2R,3S,4R,5R)-3,4,5-tris-benzyloxy-2-methanesulfonyloxy-cyclohexylmethyl ester

Guidance literature:: In pyridine; at 45 ℃; for 48h;
DOI:10.1016/0008-6215(89)85057-8

Reference yield:

: 117902-49-5
(1RS,6RS,8RS,9SR,10SR)-8,9,10-trobenzyloxy-3,3-dimethyl-2,4-dioxabicyclo<4.4.0>decane

: 125258-15-3
Benzoic acid (1S,2R,3S,4R,5R)-3,4,5-tris-benzyloxy-2-methanesulfonyloxy-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / 50percent AcOH, / ethanol; H₂O / 3.5 h / Ambient temperature

2: 83 percent / pyridine / 15 h / 40 °C

3: 83 percent / pyridine / 48 h / 45 °C

With acetic acid; In pyridine; ethanol; water;
DOI:10.1016/0008-6215(89)85057-8

Reference yield:

: 98-88-4
benzoyl chloride

: 125258-15-3
Benzoic acid (1S,2R,3S,4R,5R)-3,4,5-tris-benzyloxy-2-methanesulfonyloxy-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / pyridine / 15 h / 40 °C

2: 83 percent / pyridine / 48 h / 45 °C

In pyridine;
DOI:10.1016/0008-6215(89)85057-8