2-(4-benzyloxy-2-nitro-benzenesulfonylamino)-pentanedioic acid 1-tert-butyl ester 5-methyl ester

Base Information

Chemical Name:2-(4-benzyloxy-2-nitro-benzenesulfonylamino)-pentanedioic acid 1-tert-butyl ester 5-methyl ester
CAS No.:1053711-87-7
Molecular Formula:C₂₃H₂₈N₂O₉S
Molecular Weight:508.549
Hs Code.:

2-(4-benzyloxy-2-nitro-benzenesulfonylamino)-pentanedioic acid 1-<i>tert</i>-butyl ester 5-methyl ester

Synonyms:2-(4-benzyloxy-2-nitro-benzenesulfonylamino)-pentanedioic acid 1-tert-butyl ester 5-methyl ester

Suppliers and Price of 2-(4-benzyloxy-2-nitro-benzenesulfonylamino)-pentanedioic acid 1-tert-butyl ester 5-methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(4-benzyloxy-2-nitro-benzenesulfonylamino)-pentanedioic acid 1-tert-butyl ester 5-methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(4-benzyloxy-2-nitro-benzenesulfonylamino)-pentanedioic acid 1-tert-butyl ester 5-methyl ester

There total 4 articles about 2-(4-benzyloxy-2-nitro-benzenesulfonylamino)-pentanedioic acid 1-tert-butyl ester 5-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23577-91-5
(R)-1-tert-butyl 5-methyl 2-aminopentanedioate

: 238405-67-9
4-benzyloxy-2-nitrobenzenesulfonyl chloride

: 1053711-87-7
2-(4-benzyloxy-2-nitro-benzenesulfonylamino)-pentanedioic acid 1-tert-butyl ester 5-methyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃;
DOI:10.1021/jm020475w

Reference yield:

: 610-81-1
4-hydroxy-2-nitroaniline

: 1053711-87-7
2-(4-benzyloxy-2-nitro-benzenesulfonylamino)-pentanedioic acid 1-tert-butyl ester 5-methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium tert-butoxide / dimethylformamide / 0.5 h / 0 °C

1.2: 81 percent / dimethylformamide / 0.5 h / 0 °C

2.1: TFA; aq. HCl; NaNO₂ / 0.08 h / 0 °C

2.2: 75 percent / aq. AcOH; H₂SO₃; CuCl₂ / CuCl / 0.58 h / 20 °C

3.1: diisopropylethylamine / CH₂Cl₂ / 0 °C

With hydrogenchloride; potassium tert-butylate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium nitrite; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm020475w

Reference yield:

: 26697-35-8
4-benzyloxy-2-nitroaniline

: 1053711-87-7
2-(4-benzyloxy-2-nitro-benzenesulfonylamino)-pentanedioic acid 1-tert-butyl ester 5-methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: TFA; aq. HCl; NaNO₂ / 0.08 h / 0 °C

1.2: 75 percent / aq. AcOH; H₂SO₃; CuCl₂ / CuCl / 0.58 h / 20 °C

2.1: diisopropylethylamine / CH₂Cl₂ / 0 °C

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium nitrite; In dichloromethane;
DOI:10.1021/jm020475w