Technology Process of C24H37NO4Si
There total 16 articles about C24H37NO4Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine; hydrogen;
palladium dihydroxide;
In
1,4-dioxane; methanol;
at 20 ℃;
for 51h;
under 760.051 Torr;
DOI:10.1039/b603857c
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: (-)-sparteine; s-BuLi / diethyl ether / 5 h / -78 °C
1.2: 70 percent / diethyl ether / 1 h / -78 °C
2.1: Mg; 1,2-dibromoethane / diethyl ether / 4 h / Heating
2.2: diethyl ether / 12 h / 20 °C
3.1: aq. K2CO3; H2O2 / diethyl ether / 0.25 h / 20 °C
4.1: Et3N / CH2Cl2 / 0.5 h / cooling
5.1: 8.7 g / NaN3 / dimethylformamide / 18 h / 20 °C
6.1: pyridine; H2 / Pd(OH)2 / methanol; dioxane / 51 h / 20 °C / 760.05 Torr
With
pyridine; sodium azide; hydrogen; dihydrogen peroxide; sec.-butyllithium; potassium carbonate; magnesium; ethylene dibromide; triethylamine; (-)-sparteine;
palladium dihydroxide;
In
1,4-dioxane; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b603857c
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: 98 percent / BH3*THF / tetrahydrofuran / 21 h / 20 °C
2.1: 86 percent / DMAP / pyridine / 12 h / 90 - 100 °C
3.1: (-)-sparteine; s-BuLi / diethyl ether / 5 h / -78 °C
3.2: 70 percent / diethyl ether / 1 h / -78 °C
4.1: Mg; 1,2-dibromoethane / diethyl ether / 4 h / Heating
4.2: diethyl ether / 12 h / 20 °C
5.1: aq. K2CO3; H2O2 / diethyl ether / 0.25 h / 20 °C
6.1: Et3N / CH2Cl2 / 0.5 h / cooling
7.1: 8.7 g / NaN3 / dimethylformamide / 18 h / 20 °C
8.1: pyridine; H2 / Pd(OH)2 / methanol; dioxane / 51 h / 20 °C / 760.05 Torr
With
pyridine; dmap; sodium azide; borane-THF; hydrogen; dihydrogen peroxide; sec.-butyllithium; potassium carbonate; magnesium; ethylene dibromide; triethylamine; (-)-sparteine;
palladium dihydroxide;
In
tetrahydrofuran; 1,4-dioxane; pyridine; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b603857c