(E)-N'-(1-(3-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide

Base Information

Chemical Name:(E)-N'-(1-(3-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide
CAS No.:1220985-63-6
Molecular Formula:C₁₆H₁₈N₂O₃S
Molecular Weight:318.397
Hs Code.:

Synonyms:(E)-N'-(1-(3-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N'-(1-(3-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide

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Technology Process of (E)-N'-(1-(3-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide

There total 1 articles about (E)-N'-(1-(3-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 586-37-8
1-(3-Methoxyphenyl)ethanone

: 1220985-63-6
(E)-N'-(1-(3-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide

Guidance literature:: In methanol; at 20 ℃; for 3h;
DOI:10.1002/adsc.201900230

Reference yield: 69.0%

: 1220985-63-6
(E)-N'-(1-(3-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide

: 53256-19-2
ethyl (Z)-3-amino-3-phenylacrylate

: ethyl 5-(3-methoxyphenyl)-2-phenyl-1H-pyrrole-3-carboxylate

Guidance literature:: With tert.-butylhydroperoxide; iodine; In dimethyl sulfoxide; at 20 ℃; for 24h; Irradiation; Inert atmosphere;
DOI:10.1021/acs.joc.8b00878

Reference yield: 68.0%

: 1220985-63-6
(E)-N'-(1-(3-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide

: 5720-05-8
4-methylphenylboronic acid

: 1190931-47-5
1-methoxy-3-[1-(4-methylphenyl)vinyl]benzene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; oxygen; copper(l) chloride; lithium tert-butoxide; In 1,4-dioxane; at 70 ℃; for 7h;
DOI:10.1039/b925590g