3,4,6-tri-O-benzoyl-2-O-benzyl-β-D-glucopyranosyl thiocyanate

Base Information

Chemical Name:3,4,6-tri-O-benzoyl-2-O-benzyl-β-D-glucopyranosyl thiocyanate
CAS No.:1258410-90-0
Molecular Formula:C₃₅H₂₉NO₈S
Molecular Weight:623.683
Hs Code.:

Synonyms:3,4,6-tri-O-benzoyl-2-O-benzyl-β-D-glucopyranosyl thiocyanate

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Chemical Property of 3,4,6-tri-O-benzoyl-2-O-benzyl-β-D-glucopyranosyl thiocyanate

Chemical Property:

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Technology Process of 3,4,6-tri-O-benzoyl-2-O-benzyl-β-D-glucopyranosyl thiocyanate

There total 2 articles about 3,4,6-tri-O-benzoyl-2-O-benzyl-β-D-glucopyranosyl thiocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 72946-46-4
3,4,6-tri-O-benzoyl-2-O-benzyl-α-D-glucopyranosyl bromide

: 333-20-0
potassium thioacyanate

: 1258410-90-0
3,4,6-tri-O-benzoyl-2-O-benzyl-β-D-glucopyranosyl thiocyanate

Guidance literature:: With 18-crown-6 ether; In acetone; at 20 ℃; for 2.5h; Inert atmosphere;
DOI:10.1021/ol1023079

Reference yield:

: 1,3,4,6-tetra-O-benzoyl-2-O-benzyl-D-glucopyranose

: 1258410-90-0
3,4,6-tri-O-benzoyl-2-O-benzyl-β-D-glucopyranosyl thiocyanate

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; Acetyl bromide / dichloromethane / 2 h / 0 °C

2: 18-crown-6 ether / acetone / 2.5 h / 20 °C / Inert atmosphere

With methanol; 18-crown-6 ether; Acetyl bromide; In dichloromethane; acetone;
DOI:10.1021/ol1023079

Reference yield:

: 53008-65-4,641635-63-4
methyl 2,3,4-tri-O-benzyl-D-glucopyranoside

: 1258410-90-0
3,4,6-tri-O-benzoyl-2-O-benzyl-β-D-glucopyranosyl thiocyanate

: methyl 2-O-benzyl-3, 4, 6-tri-O-benzoyl-D-glucopyranosyl-β-(1→6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

: 1233488-82-8
methyl 2-O-benzyl-3, 4, 6-tri-O-benzoyl-D-glucopyranosyl-α-(1→6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: With copper(II) bis(trifluoromethanesulfonate); In 1,2-dichloro-ethane; at 20 ℃; for 1h; optical yield given as %de; stereoselective reaction; Molecular sieve;
DOI:10.1021/ol1023079