7-ethoxy-carbonylmethoxyflavanone

Base Information

• Chemical Name: 7-ethoxy-carbonylmethoxyflavanone
• CAS No.: 2430-55-9
• Molecular Formula: C₁₉H₁₈O₅
• Molecular Weight: 326.349
• Mol file: 2430-55-9.mol

Synonyms:7-ethoxy-carbonylmethoxyflavanone

Chemical Property of 7-ethoxy-carbonylmethoxyflavanone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 7-ethoxy-carbonylmethoxyflavanone

There total 2 articles about 7-ethoxy-carbonylmethoxyflavanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.9%

ethyl bromoacetate (105-36-2) + 7-hydroxy-2-phenyl-chroman-4-one (6515-36-2,2545-13-3) → 7-ethoxy-carbonylmethoxyflavanone (2430-55-9)

Guidance literature:

With potassium carbonate; In acetone; at 59.9 - 64.9 ℃; for 8h; Heating;

DOI:10.1107/S0108270195002940

Reference yield:

ethyl bromoacetate (105-36-2) → 7-ethoxy-carbonylmethoxyflavanone (2430-55-9)

Guidance literature:

With potassium carbonate; acetone;

Reference yield:

7-ethoxy-carbonylmethoxyflavanone (2430-55-9) → 7-ethoxycarbonylmethoxyflavone (119-41-5)

Guidance literature:

Multi-step reaction with 2 steps

1: N-bromo-succinimide; dibenzoyl peroxide; chloroform / Erwaermen des Reaktionsprodukts mit wss.-aethanol. Natronlauge

2: sulfuric acid; ethanol

With N-Bromosuccinimide; ethanol; chloroform; sulfuric acid; dibenzoyl peroxide;

upstream raw materials:

ethyl bromoacetate

7-hydroxy-2-phenyl-chroman-4-one

Downstream raw materials:

2-((4-oxo-2-phenyl-4H-chromen-7-yl)oxy)acetic acid

7-ethoxycarbonylmethoxyflavone